金属热处理 ›› 2025, Vol. 50 ›› Issue (11): 146-153.DOI: 10.13251/j.issn.0254-6051.2025.11.021

• 组织与性能 • 上一篇    下一篇

核电用GH3625合金棒材的组织与性能

王绍灼, 李燕, 荣若平, 樊海卫, 唐超, 杨萍   

  1. 山东昱锟高合新材料有限公司, 山东 淄博 255000
  • 收稿日期:2025-06-07 修回日期:2025-10-01 发布日期:2025-12-16
  • 作者简介:王绍灼(1982—),男,高级工程师,硕士,主要研究方向为航空、航天、核电等领域用高温合金、钛合金材料工艺,E-mail:wangshaozhuo@126.com

Microstructure and mechanical properties of GH3625 alloy bars for nuclear power

Wang Shaozhuo, Li Yan, Rong Ruoping, Fan Haiwei, Tang Chao, Yang Ping   

  1. Shandong Yukun Gaohe New Material Co., Ltd., Zibo Shandong 255000, China
  • Received:2025-06-07 Revised:2025-10-01 Published:2025-12-16

摘要: 通过真空感应熔炼、氩气保护电渣重熔、锻造和热处理试制核电用GH3625合金ϕ148 mm和ϕ84 mm棒材,对固溶态合金进行显微组织、室温/高温拉伸、高温持久蠕变测试,对固溶+时效态合金进行显微组织及韧性表征。结果表明,ϕ148 mm和ϕ84 mm棒材固溶态显微组织均为单相奥氏体、双重晶粒,ϕ84 mm棒材晶粒略细。随时效时间延长,晶粒不均匀性程度增加,780 ℃时效后晶粒较细小,但碳化物析出严重。固溶态ϕ84 mm棒材室温拉伸强度比ϕ148 mm高,塑性相当,高温拉伸性能优于ϕ148 mm,随拉伸试验温度升高,强度呈现明显降低趋势,断面收缩率呈上升趋势,伸长率先升后降。ϕ148 mm固溶态棒材在780 ℃/150 MPa和920 ℃/45 MPa试验条件下蠕变断裂时间为857 h和244 h,高温持久塑性较好。560 ℃时效后,ϕ148 mm棒材冲击吸收能量均大于300 J,780、920 ℃下,随时效时间延长,冲击吸收能量连续降低,780 ℃时效后合金的冲击性能最差。

关键词: GH3625合金棒材, 固溶处理, 时效, 显微组织, 拉伸性能, 高温持久性能, 冲击性能

Abstract: Through vacuum induction melting, argon-shielded electroslag remelting, forging and heat treatment, the GH3625 alloy bars with diameter of 148 mm and 84 mm for nuclear power were trial produced. The microstructure, room and elevated temperature tensile tests, high-temperature rupture and creep tests were conducted on the bars under solution treated state, and then the microstructure and toughness characteristics were conducted on the bars solution treated and aged. The results show that both the microstructures of the bars with diameter of 148 mm and 84 mm are single-phase austenite with duplex grain sizes, and the average grain size of the bar with diameter of 84 mm is slightly smaller. The inhomogeneity of grain increases with the extension of aging time. The grain size aged at 780 ℃ is finer, but the precipitation of carbides is more serious at the same time. The room-temperature tensile strength of the bar with diameter of 84 mm is higher than that of 148 mm, and the plasticity is equivalent between the two; the high-temperature tensile properties of the bar with diameter of 84 mm is generally better than that of 148 mm. With the increase of tensile test temperatures, the tensile strength shows a significant decrease trend, the percentage reduction of area shows an upward trend, and the elongation ascends firstly and then descends. The creep rupture life of the bar with diameter of 148 mm is 857 h and 244 h under the test conditions of 780 ℃/150 MPa and 920 ℃/45 MPa, which means good high-temperature creep plasticity. The impact absorbed energy of the bar aged at 560 ℃ is greater than 300 J, which decreases continuously as the aging time increases at 780 ℃ and 920 ℃, and the impact property of the bar aged at 780 ℃ is the poorest.

Key words: GH3625 alloy bars, solution treatment, aging, microstructure, tensile properties, high-temperature rupture properties, impact property

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