金属热处理 ›› 2026, Vol. 51 ›› Issue (2): 211-217.DOI: 10.13251/j.issn.0254-6051.2026.02.031

• 工艺研究 • 上一篇    下一篇

等温淬火对低温用18Ni(200)马氏体时效钢组织与性能的影响

胡继康1, 殷立涛2, 李洲1, 邓想涛3, 徐流杰1   

  1. 1.河南科技大学 材料科学与工程学院, 河南 洛阳 471003;
    2.洛阳中重铸锻有限责任公司, 河南 洛阳 471039;
    3.东北大学 轧制技术及连轧自动化国家重点实验室, 辽宁 沈阳 110819
  • 收稿日期:2025-09-10 修回日期:2025-12-19 发布日期:2026-03-05
  • 通讯作者: 徐流杰,教授,博士,E-mail:wmxlj@126.com
  • 作者简介:胡继康(1999—),男,硕士研究生,主要研究方向为低温用马氏体时效钢,E-mail:h18439399513@163.com。
  • 基金资助:
    河南省重点研发专项(231111230400);国家重点研发计划(2022YFB3705300)

Effect of austempering on microstructure and properties of maraging steel for low temperature environment

Hu Jikang1, Yin Litao2, Li Zhou1, Deng Xiangtao3, Xu Liujie1   

  1. 1. School of Materials Science and Engineering, Henan University of Science and Technology, Luoyang Henan 471003, China;
    2. Luoyang CITIC HIC Casting & Forging Co., Ltd., Luoyang Henan 471039, China;
    3. State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang Liaoning 110819, China
  • Received:2025-09-10 Revised:2025-12-19 Published:2026-03-05

摘要: 针对18Ni(200)马氏体时效钢强韧性协同调控难题,提出1000 ℃×1 h固溶+800 ℃×1 h固溶+230 ℃×8 h等温淬火+500 ℃×3 h时效的复合工艺。通过对比传统工艺(1000 ℃×1 h固溶+800 ℃×1 h固溶+-196 ℃×1 h深冷+500 ℃×3 h时效),研究了等温淬火对18Ni(200)钢显微组织和力学性能的影响。结果表明,固溶处理后经等温淬火,将板条马氏体转变为超细贝氏体,再经时效处理后,形成了贝氏体和少量(2.5%)逆转变奥氏体复合组织,并生成大量纳米析出相。与传统工艺中马氏体板条块宽度(16.3 μm)相比,贝氏体板条宽度(3.4 μm)显著细化。等温淬火试样抗拉强度、屈服强度和-196 ℃冲击吸收能量分别达到(1573±15) MPa、(1432±17) MPa和(15±2) J,较传统工艺分别提高了14.5%、18.7%和87.5%。断口分析表明,等温淬火试样的低温断裂模式为准解理型,与传统工艺钢相比,韧窝大小及数量显著增加。贝氏体细晶强韧化、逆转变奥氏体TRIP效应与纳米析出相协同作用是18Ni(200)强韧性提升的原因。

关键词: 马氏体时效钢, 等温淬火, 超细贝氏体, 逆转变奥氏体, 力学性能

Abstract: To address the challenge of synergistic strength-toughness regulation in 18Ni(200) maraging steel, a composite process involving 1000 ℃×1 h solution treatment + 800 ℃×1 h solution treatment + 230 ℃×8 h austempering + 500 ℃×3 h aging was proposed. Through comparative studies with the traditional process (1000 ℃×1 h solution treatment + 800 ℃×1 h solution treatment + -196 ℃×1 h cryogenic treatment + 500 ℃×3 h aging), effects of austempering on microstructure and mechanical properties of the 18Ni(200) steel were investigated. The results indicate that after solution treatment, by austempering lath martensite is transformed into ultrafine bainite, further by aging, a composite structure of bainite and a small amount (2.5%) of reversed austenite is formed, accompanied by abundant nano-sized precipitates. Compared with the martensite block width (16.3 μm) in the conventional process, the bainite lath width (3.4 μm) is significantly refined. The tensile strength, yield strength, and -196 ℃ impact absorbed energy of the austempered specimen reach (1573±15) MPa, (1432±17) MPa, and (15±2) J, respectively, which are 14.5%, 18.7%, and 87.5% higher than those of traditional processes. Fracture analysis shows that the low-temperature fracture mode of the austempered specimen is quasi cleavage type. Compared with traditional process treated steel, the size and number of toughness dimples are significantly increased. The synergistic effect of bainite fine grain strengthening, reverse austenite TRIP effect, and nano precipitation is the reason for the improvement of strength and toughness of the 18Ni (200) steel.

Key words: maraging steel, austempering, ultrafine bainite, reversed austenite, mechanical properties

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