金属热处理 ›› 2025, Vol. 50 ›› Issue (11): 253-259.DOI: 10.13251/j.issn.0254-6051.2025.11.035

• 工艺研究 • 上一篇    下一篇

热处理工艺对选区激光熔化TC4钛合金中α′相转变的影响

温钟淳1, 李明1, 郑建超1, 金冬岩1, 赵栋1, 陈璨2   

  1. 1.沈阳飞机工业(集团)有限公司 钛合金加工中心, 辽宁 沈阳 110850;
    2.湖南华曙高科技股份有限公司, 湖南 长沙 410205
  • 收稿日期:2025-07-04 修回日期:2025-10-08 发布日期:2025-12-16
  • 作者简介:温钟淳(1998—),男,工程师,主要研究方向为增材制造成形,E-mail:18540105622@163.com

Effect of heat treatment process on α′ phase transformation in selective laser melted TC4 titanium alloy

Wen Zhongchun1, Li Ming1, Zheng Jianchao1, Jin Dongyan1, Zhao Dong1, Chen Can2   

  1. 1. Titanium Machining Center, Shenyang Aircraft Corporation, Shenyang Liaoning 110850, China;
    2. Farsoon Technologies Co., Ltd., Changsha Hunan 410205, China
  • Received:2025-07-04 Revised:2025-10-08 Published:2025-12-16

摘要: 使用选区激光熔化技术(SLM)制备TC4钛合金试样,利用光学显微镜及万能试验机研究了热处理条件对显微组织中α′相转变及力学性能的影响。结果表明:沉积态TC4合金宏观组织为外延生长的β柱状晶,微观组织由大量α′相、α相以及弥散分布的β相组成。随着退火温度升高,β相溶解度逐渐变小,α′相发生β转变的倾向逐渐变大,同时α相粗化更为明显。当固溶温度为900 ℃时,α′相几乎完全分解,组织内存在大量过饱和的亚稳β相。随着时效温度提高,析出的次生α相数量更多,形状逐渐从针状变为片层状。合金的力学性能整体上呈现出强度降低、断后伸长率升高的趋势。经过对比,900 ℃×1 h(AC)固溶+500 ℃×2 h(AC)时效处理后的TC4合金综合力学性能最佳。

关键词: 选区激光熔化, 钛合金, 热处理, α′相, 拉伸性能

Abstract: TC4 titanium alloy specimens were prepared by using selective laser melting (SLM) technology, and the effect of heat treatment conditions on the α′ phase transformation in microstructure and mechanical properties was investigated by using optical microscope and universal testing machine. The results show that the macroscopic structure of the deposited TC4 alloy is epitaxial β columnar crystal, and the microstructure consists of a large number of α′ phases, α phases, and dispersed β phases. As the annealing temperature increases, the solubility of β phase gradually becomes smaller, the tendency of β transformation of α′ phase gradually becomes larger, and the coarsening of α phase is more obvious. When the solution treatment temperature is 900 ℃, α′ phase is almost completely decomposed, and there are a large number of supersaturated metastable β phases. With the increase of aging temperature, the amount of precipitated secondary α phase is more, and the shape gradually changes from needle-like to lamellar. The mechanical properties of the alloy generally exhibit a trend of decreasing strength and increasing elongation. After comparison, the comprehensive mechanical properties of the TC4 alloy solution treated at 900 ℃ for 1 h(AC) and aged at 500 ℃ for 2 h(AC) are the best.

Key words: selective laser melting, titanium alloy, heat treatment, α′ phase, tensile properties

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