金属热处理 ›› 2026, Vol. 51 ›› Issue (2): 257-265.DOI: 10.13251/j.issn.0254-6051.2026.02.038

• 工艺研究 • 上一篇    下一篇

热处理工艺对增材制造Ti31钛合金微观组织与力学性能的影响

陈浩瀚, 蒋文天, 盖欣, 丁涛, 龚亚, 付超   

  1. 中国核动力研究设计院, 四川 成都 610213
  • 收稿日期:2025-11-05 修回日期:2025-12-04 发布日期:2026-03-05
  • 作者简介:陈浩瀚(1996—),男,助理研究员,硕士,主要从事增材制造工艺研究,E-mail:chenhaohan@npic.ac.cn
  • 基金资助:
    稳定支持科研计划(WDZC-2023-05-03-03)

Effect of heat treatment on microstructure and mechanical properties of additive manufactured Ti31 titanium alloy

Chen Haohan, Jiang Wentian, Gai Xin, Ding Tao, Gong Ya, Fu Chao   

  1. Nuclear Power Institute of China, Chengdu Sichuan 610213, China
  • Received:2025-11-05 Revised:2025-12-04 Published:2026-03-05

摘要: 利用扫描电镜、电子背散射衍射、X射线衍射仪、拉伸试验机和冲击试验机研究了热处理工艺对增材制造Ti31钛合金微观组织和力学性能的影响。结果表明,沉积态Ti31钛合金的组织为针状马氏体,800 ℃+炉冷处理后合金组织为细条状α相以及少量块状α相,800 ℃+空冷处理合金的组织为细条状α相,900 ℃+空冷处理合金的组织为细条状α相及少量等轴α相,900 ℃+空冷-800 ℃+空冷双重热处理后合金的组织为板条状α相及部分等轴α相。不同热处理工艺下合金均表现出相同取向的织构,均在[0001]基面呈现最大的织构强度。随着热处理冷却速率的减小和热处理次数的增加,SLM Ti31钛合金的抗拉强度降低;随着热处理温度和热处理次数的增加,SLM Ti31钛合金的伸长率提升。800 ℃+炉冷处理的SLM Ti31钛合金由于块状α相的产生,表现出较差的冲击性能。800 ℃+空冷处理后的SLM Ti31钛合金的抗拉强度可达840 MPa,伸长率为20.3%,冲击吸收能量为75.9 J,综合力学性能最好。

关键词: Ti31钛合金, 增材制造, 热处理, 显微组织, 力学性能

Abstract: Effect of heat treatment on the microstructure and mechanical properties of the additive manufactured T31 titanium alloy was investigated by means of scanning electron microscope, electron backscatter diffraction, X-ray diffractometer, tensile testing machine and impact testing machine. The results indicate that the microstructure of the as-deposited Ti31 titanium alloy is acicular martensite. After annealing at 800 ℃ followed by furnace cooling, the microstructure is composed of fine strip-like α phase and a small amount of bulk α phase. After annealing at 800 ℃ followed by air cooling, the microstructure is fine strip-like α phase. The microstructure of the alloy annealed at 900 ℃ followed by air cooling consists of fine lath-like α phase and a small amount of equiaxed α phase, while the microstructure after dual heat treatment of annealing at 900 ℃ followed by air cooling and annealing at 800 ℃ followed by air cooling comprises lath-like α phase and partial equiaxed α phase. All alloys subjected to different heat treatments exhibit texture of the same orientation, with the maximum texture intensity observed in the [0001] basal plane. With the increase in number of heat treatments and decrease in cooling rate, the tensile strength of the SLM Ti31 titanium alloy decreases; with the increase in heat treatment temperature and number of heat treatments, the elongation of the alloy improves. The SLM Ti31 titanium alloy annealed at 800 ℃ followed by furnace cooling exhibits poor impact property due to the formation of bulk α phase. After annealing at 800 ℃ followed by air cooling, the tensile strength of the SLM Ti31 titanium alloy can reach 840 MPa, with an elongation of 20.3% and an impact absorbed energy of 75.9 J, demonstrating the optimal comprehensive mechanical properties.

Key words: T31 titanium alloy, additive manufacturing, heat treatment, microstructure, mechanical properties

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