金属热处理 ›› 2025, Vol. 50 ›› Issue (6): 294-296.DOI: 10.13251/j.issn.0254-6051.2025.06.045

• 表面工程 • 上一篇    下一篇

基片温度对真空蒸镀铝薄膜组织及附着力的影响

张倩, 李继高   

  1. 武汉文理学院 智能制造与无损检测学院, 湖北 武汉 430345
  • 收稿日期:2024-12-23 修回日期:2025-03-27 出版日期:2025-06-25 发布日期:2025-07-08
  • 通讯作者: 李继高,副教授,硕士,E-mail: 348719689@qq.com
  • 作者简介:张 倩(1989—),女,讲师,硕士,主要研究方向为材料工程,E-mail: zqian202306@163.com。

Effect of substrate temperature on microstructure and adhesion of vacuum vapor-deposited Al films

Zhang Qian, Li Jigao   

  1. School of Intelligent Manufacturing and Non-Destructive Testing, Wuhan College of Arts and Sciences, Wuhan Hubei 430345, China
  • Received:2024-12-23 Revised:2025-03-27 Online:2025-06-25 Published:2025-07-08

摘要: 采用真空蒸镀法在不同温度的基片表面制备铝薄膜,并对其进行真空退火处理。通过X射线衍射仪(XRD)、扫描电镜(SEM)、剥离法等研究了基片温度(25、150、200 ℃)对Al薄膜组织结构及附着力的影响。结果表明,基片温度过高或过低都会导致Al薄膜生长不均匀。基片温度为150 ℃时,Al薄膜晶粒尺寸大小均匀,为合适的基片温度。提高基片温度有利于提高薄膜的附着力,但提高的幅度不大。

关键词: 基片温度, Al薄膜, 退火, 晶粒, 附着力

Abstract: Al thin films were prepared on substrates with different temperatures by the vacuum evaporation method, and then vacuum annealing treatment was carried out on them. The effect of substrate temperature (25, 150, 200 ℃) on the microstructure and adhesion of the Al thin films were studied by means of X-ray diffractometer (XRD), scanning electron microscope (SEM), the peeling method, etc. The results show that when the substrate temperature is too high or too low, the growth of the Al thin films is uneven. When the substrate temperature is 150 ℃, the grain size of the Al thin film is uniform, indicating that this is an appropriate substrate temperature. Increasing the substrate temperature is beneficial to improve the adhesion of the thin film, but the improvement range is not large.

Key words: substrate temperature, Al film, annealing, grain, adhesion

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