金属热处理 ›› 2025, Vol. 50 ›› Issue (6): 79-88.DOI: 10.13251/j.issn.0254-6051.2025.06.013

• 组织与性能 • 上一篇    下一篇

加热温度和保温时间对P20模具钢奥氏体晶粒长大与马氏体相变的影响

戴本尧1, 袁清2, 李忠波3, 包琳琳2   

  1. 1.浙江工贸职业技术学院, 浙江 温州 325000;
    2.武汉科技大学 先进耐火材料全国重点实验室, 湖北 武汉 430081;
    3.南阳汉冶特钢有限公司, 河南 南阳 474571
  • 收稿日期:2025-01-03 修回日期:2025-04-20 出版日期:2025-06-25 发布日期:2025-07-08
  • 通讯作者: 袁 清,副教授,博士,E-mail: yuanqing@wust.edu.cn
  • 作者简介:戴本尧(1980—),男,高级实验师,硕士,主要研究方向为电机一体化、材料开发,E-mail: 16920491@qq.com。
  • 基金资助:
    国家自然科学基金(52004193);湖北省自然科学基金一般面上项目(2024AFB900)

Influence of heating temperature and holding time on austenite grain growth and martensitic transformation of P20 die steel

Dai Benyao1, Yuan Qing2, Li Zhongbo3, Bao Linlin2   

  1. 1. Zhejiang Industry & Trade Vocational College, Wenzhou Zhejiang 325000, China;
    2. State Key Laboratory of Advanced Refractories, Wuhan University of Science and Technology, Wuhan Hubei 430081, China;
    3. Nanyang Hanye Special Steel Co. Ltd., Nanyang Henan 474571, China
  • Received:2025-01-03 Revised:2025-04-20 Online:2025-06-25 Published:2025-07-08

摘要: 利用高温激光共聚焦显微镜对不同加热温度(850~1200 ℃)和保温时间下的P20模具钢奥氏体晶粒长大和马氏体相变进行了原位观察。结果表明,P20模具钢奥氏体晶粒对加热温度有极高的敏感性。随加热温度升高,平均奥氏体晶粒尺寸增大,由850 ℃时的18.82 μm增加至1200 ℃时的126.89 μm。在900 ℃和1200 ℃均出现了急剧增大现象,这是因为900 ℃以碳化物发生球化为主,而1200 ℃时碳化物颗粒以回溶为主,这两种碳化物演变均削弱了奥氏体晶界的钉扎效果。此外,奥氏体晶粒尺寸增大可促进马氏体相变,马氏体相变开始温度从263.2 ℃(加热温度850 ℃时)提高至335.9 ℃(加热温度1200 ℃时)。马氏体相变呈现出选择性启动模式,并非全部为爆发式形核和长大特征。另外,过冷奥氏体在冷却过程中形成新鲜马氏体和二次马氏体,二次马氏体依附于新鲜马氏体形成,与新鲜马氏体呈典型60°夹角。

关键词: 模具钢, 加热温度, 保温时间, 奥氏体晶粒长大, 马氏体相变

Abstract: Austenite grain growth and martensitic transformation of P20 die steel under different heating temperatures (850-1200 ℃) and holding time were investigated via in situ observation using a high-temperature laser scanning confocal microscope. The results demonstrate that austenite grains of the P20 die steel exhibit extremely high sensitivity to heating temperature. As the heating temperature increases, the average austenite grain size significantly enlarges, rising from 18.82 μm at 850 ℃ to 126.89 μm at 1200 ℃. Notably, abrupt grain growth occurs at both 900 ℃ and 1200 ℃. This phenomenon is attributed to that the spheroidization of carbides is dominant at 900 ℃, while the dissolution of carbide particles is predominant at 1200 ℃, both of which reduce pinning effect on austenite grain boundaries. Additionally, the increase of austenite grain size promotes martensitic transformation, with the martensite start temperature (Ms) increasing from 263.2 ℃ (heated at 850 ℃) to 335.9 ℃ (heated at 1200 ℃). The martensitic transformation follows a selective initiation mode, rather than exhibiting fully explosive nucleation and growth. Furthermore, during cooling, under cooled austenite forms fresh martensite and secondary martensite. The secondary martensite nucleates and grows adjacent to the fresh martensite, typically forming approximately 60° angles with the fresh martensite.

Key words: die steel, heating temperature, holding time, austenite grain growth, martensitic transformation

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