金属热处理 ›› 2025, Vol. 50 ›› Issue (5): 195-201.DOI: 10.13251/j.issn.0254-6051.2025.05.030

• 工艺研究 • 上一篇    下一篇

QPQ渗氮温度对32Cr3MoVE钢组织与性能的影响

辛昕1, 张宇慧1, 周锴1, 范鹏举2, 金国2   

  1. 1.中国航发哈尔滨东安发动机有限公司, 黑龙江 哈尔滨 150066;
    2.哈尔滨工程大学 材料科学与化学工程学院, 黑龙江 哈尔滨 150001
  • 收稿日期:2024-11-24 修回日期:2025-03-13 发布日期:2025-06-25
  • 通讯作者: 金 国,教授,博士,E-mail:jinjg721@163.com
  • 作者简介:辛 昕(1983—),女,高级工程师,硕士,主要研究方向为金属材料热处理,E-mail:18145626894@163.com。
  • 基金资助:
    中国航发哈尔滨东安发动机有限公司-液态氮化表面增强技术研究项目(DCGY230006)

Effect of QPQ nitriding temperature on microstructure and properties of 32Cr3MoVE steel

Xin Xin1, Zhang Yuhui1, Zhou Kai1, Fan Pengju2, Jin Guo2   

  1. 1. AECC Harbin Dong'an Engine Co., Ltd., Harbin Heilongjiang 150066, China;
    2. College of Materials Science and Chemical Engineering, Harbin Engineering University, Harbin Heilongjiang 150001, China
  • Received:2024-11-24 Revised:2025-03-13 Published:2025-06-25

摘要: 对齿轮用32Cr3MoVE钢进行560 ℃不同渗氮时间(90、120、150 min)下的QPQ处理,并对其物相组成、渗层形貌、显微硬度、耐磨性能和耐蚀性能进行了测试。结果表明,不同渗氮时间QPQ处理后,渗层由Fe2N、Fe3N及Fe3O4相组成,其中90、120 min渗氮试样主相为Fe3N相,150 min渗氮试样主相为Fe2N相。随渗氮时间延长,化合物层厚度增加。渗氮时间120 min QPQ处理试样的硬度最高(932.4 HV0.1),耐磨性最好,干摩擦下磨损量仅2.2 mg,且耐蚀性最好,电流密度最低,极化曲线出现钝化区,推测其在腐蚀过程中形成包含金属氧化物的钝化膜,延缓了腐蚀速率。

关键词: QPQ处理, 渗氮时间, 32Cr3MoVE钢, 渗氮层形貌, 硬度, 耐磨性, 耐蚀性

Abstract: QPQ treatment was carried out on 32Cr3MoVE steel for gears at 560 ℃ for different nitriding time (90, 120, 150 min), and its phase composition, nitrided layer morphology, microhardness, wear resistance, and corrosion resistance were tested. The results show that the nitrided layer is composed of Fe2N, Fe3N and Fe3O4 phases after QPQ treatment for different nitriding time. The main phase of the nitrided specimens for 90 min and 120 min is Fe3N, while the main phase of the specimen nitrided for 150 min is Fe2N. With the extension of nitriding time, the thickness of the compound layer increases. The specimen QPQ nitrided for 120 min has the highest hardness (932.4 HV0.1), the best wear resistance with wear loss of only 2.2 mg at dry friction, and the best corrosion resistance, with the lowest current density, and a passivation zone appearing in the polarization curve which is speculated to form a passivation film containing metal oxides during the corrosion process, and that delays the corrosion rate.

Key words: QPQ processing, nitriding time, 32Cr3MoVE steel, nitrided layer morphology, hardness, abrasion resistance, corrosion resistance

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