Inconel 625合金组织与性能的模拟计算与高通量试验

doi:10.13251/j.issn.0254-6051.2025.08.027

金属热处理 ›› 2025, Vol. 50 ›› Issue (8): 169-176.DOI: 10.13251/j.issn.0254-6051.2025.08.027

Inconel 625合金组织与性能的模拟计算与高通量试验

刘文月^1,2, 李天怡^1,2, 巩俐^1,2, 任毅^1,3, 杨博威^1,2, 安涛^1,2

1.海洋装备金属材料及其应用全国重点实验室, 辽宁鞍山 114009;
2.鞍钢集团北京研究院有限公司, 北京 102200;
3.鞍钢股份有限公司, 辽宁鞍山 114021

收稿日期:2025-02-12 修回日期:2025-06-18 出版日期:2025-08-25 发布日期:2025-09-10
作者简介:刘文月(1980—),男,正高级工程师,博士,主要研究方向为高强韧中厚板材料开发与工艺,E-mail:liuwenyue@ansteel.com.cn

Computational simulation and high-throughput experiment on microstructure and properties of Inconel 625 alloy

Liu Wenyue^1,2, Li Tianyi^1,2, Gong Li^1,2, Ren Yi^1,3, Yang Bowei^1,2, An Tao^1,2

1. State Key Laboratory of Metallic Materials for Marine Equipment and Applications, Anshan Liaoning 114009, China;
2. Ansteel Beijing Research Institute Co., Ltd., Beijing 102200, China;
3. Angang Steel Co., Ltd., Anshan Liaoning 114021, China

Received:2025-02-12 Revised:2025-06-18 Online:2025-08-25 Published:2025-09-10

摘要/Abstract

摘要： 基于Thermo-Calc热力学模拟软件、光学显微镜、扫描电镜、能谱仪、拉伸试验机等,对Inconel 625合金进行了组织与性能的模拟计算和高通量试验,研究了Inconel 625合金铸态、轧态及热处理态试样的显微组织、力学性能与耐蚀性。结果表明,Inconel 625合金的铸态显微组织为树枝晶,枝晶间可见Ni₃Nb相分布及明显的Mo、Nb成分偏析。铸态、热轧态、调质态及固溶态Inconel 625合金的微观组织基本一致,均为γ基体与Ni₃Nb相构成的混合组织,主要区别在于Ni₃Nb相的含量。成分偏析对合金的耐蚀性影响显著。经3种轧前热处理方式对比,轧前1250 ℃保温3 h即可获得较好的成分均匀化效果。对比3种轧后热处理方式,调质能获得较好的强度-塑性-耐蚀性的综合匹配。推荐21.5Cr-9Mo-3.65Nb为生产Inconel 625/X65复合板的Inconel 625合金参考成分。

关键词: 镍基合金, Thermo-Calc, 高通量试验, 微观组织, 微观偏析, 耐蚀性

Abstract: Based on Thermo-Calc thermodynamic simulation software, optical microscope, scanning electron microscope, energy dispersive spectrometer, tensile testing machine, etc., the microstructure and properties of the Inconel 625 alloy were simulated and subjected to high-throughput experiment. The microstructure, mechanical properties, and corrosion resistance of the Inconel 625 alloy as-cast, hot rolled, and heat treated specimens were studied. The results indicate that the as-cast microstructure of the Inconel 625 alloy is dendritic, with visible distribution of Ni₃Nb phase and significant segregation of Mo and Nb elements between dendrites. The microstructure of the Inconel 625 alloy as-cast, hot rolled, quenched and tempered, and solution treated is basically the same, consisting of a mixed structure of γ matrix and Ni₃Nb phase, with the main difference being the content of Ni₃Nb phase. The segregation of components has a significant impact on the corrosion resistance of alloy. After comparing three heat treatment methods before hot rolling, it is found that a better homogenization effect can be achieved by holding at 1250 ℃ for 3 h before rolling. Comparing three post rolling heat treatment methods, quenching and tempering can achieve a better comprehensive matching of strength, plasticity, and corrosion resistance. The composition of 21.5Cr-9Mo-3.65Nb is recommended as the Inconel 625 alloy reference composition for producing Inconel 625/X65 composite plate.

Key words: nickel based alloy, Thermo-Calc, high-throughput experiment, microstructure, micro-segregation, corrosion resistance

中图分类号:

刘文月, 李天怡, 巩俐, 任毅, 杨博威, 安涛. Inconel 625合金组织与性能的模拟计算与高通量试验[J]. 金属热处理, 2025, 50(8): 169-176.

Liu Wenyue, Li Tianyi, Gong Li, Ren Yi, Yang Bowei, An Tao. Computational simulation and high-throughput experiment on microstructure and properties of Inconel 625 alloy[J]. Heat Treatment of Metals, 2025, 50(8): 169-176.

参考文献

[1] Tachibana S, Kuronuma Y, Yokota T, et al. Effect of hot rolling and cooling conditions on intergranular corrosion behavior in Alloy625 clad steel[J]. Corrosion Science, 2015, 99: 125-133.
[2] Tsuji M, Kobayashi Y, Kitada T, et al. High nickel alloy clad pipe by UOE process for H₂S-CO₂-Cl environment[C]//Seventh International Conference on Offshore Mechanics and Arctic Engineering, Houston, Texas. 1988: 221-228.
[3] Tachibana S, Kuronuma Y, Yokota T, et al. Development of TMCP type Alloy 625/X65 clad steel plate for pipe[C]//International Pipeline Conference. American Society of Mechanical Engineers, 2014.
[4] Ganesan P, Renteria C M, Crum J R. Versatile corrosion resistance of Inconel alloy 625 in various aqueous and chemical processing environments[J]. Superalloys, 1991, 718: 663-680.
[5] Stevens C E, Ross R W. Production, fabrication, and performance of alloy 625 clad steel for aggressive corrosive environments[J]. Journal of Materials for Energy Systems, 1986, 8(1): 7-16.
[6] 杨鹏辉, 杜琳琳, 王蓉, 等. Inconel 625合金国内外研究现状综述[J]. 铸造技术, 2023, 44(4): 322-331.
Yang Penghui, Du Linlin, Wang Rong, et al. Review of the current status of domestic and international research on Inconel 625 alloy[J]. Foundry Technology, 2023, 44(4): 322-331.
[7] 王浩宇, 董建新, 张麦仓, 等. 浇铸温度对GH625合金铸态显微组织的影响[J]. 工程科学学报, 2015, 37(11): 1469-1476.
Wang Haoyu, Dong Jianxin, Zhang Maicang, et al. Effect of casting temperature on the microstructure of as-cast GH625 alloy[J]. Chinese Journal of Engineering, 2015, 37(11): 1469-1476.
[8] 孙锋, 梅林波, 刘松锋, 等. 625合金凝固偏析的理论分析[J]. 热力透平, 2016, 45(1): 46-50.
Sun Feng, Mei Linbo, Liu Songfeng, et al. Theoretic analysis on solidification segregation of alloy 625[J]. Thermal Turbine, 2016, 45(1): 46-50.
[9] 丁雨田, 王伟, 李海峰, 等. GH3625合金中析出相的热力学计算[J]. 兰州理工大学学报, 2016, 42(5): 1-5.
Ding Yutian, Wang Wei, Li Haifeng, et al. Thermodynamic calculation of precipitated phases in alloy GH3625[J]. Journal of Lanzhou University of Technology, 2016, 42(5): 1-5.
[10] 丁雨田, 豆正义, 高钰璧, 等. 原位观察不同冷却速率下GH3625合金的凝固过程[J]. 材料导报B: 研究篇, 2017, 31(12): 150-155.
Ding Yutian, Dou Zhengyi, Gao Yubi, et al. In-situ observation of solidification process of GH3625 superalloy at different cooling rates[J]. Materials Reports, 2017, 31(12): 150-155.
[11] Barella S, Gruttadauria A, Mapelli C, et al. Solidification microstructure of centrifugally cast Inconel 625[J]. China Foundry, 2017, 14: 304-312.
[12] 胡显军, 孙丹丹, 张珂, 等. 固溶温度对热轧Inconel625合金组织与力学性能的影响[J]. 材料热处理学报, 2019, 40(9): 64-69.
Hu Xianjun, Sun Dandan, Zhang Ke, et al. Effect of solution temperature on microstructure and mechanical properties of hot rolled Inconel625 alloy[J]. Transactions of Materials and Heat Treatment, 2019, 40(9): 64-69.
[13] 丁雨田, 豆正义, 高钰璧, 等. 均匀化GH3625合金熔化和凝固过程中的相变[J]. 材料研究学报, 2017, 31(11): 853-859.
Ding Yutian, Dou Zhengyi, Gao Yubi, et al. Phase transformation during melting and solidifying process of homogenized superalloy GH3625[J]. Chinese Journal of Materials Research, 2017, 31(11): 853-859.
[14] 黄健成, 姚润钢, 姚上卫. 镍基625合金的析出转变及影响因素[J]. 材料开发与应用, 2016, 31(1): 87-91.
Huang Jiancheng, Yao Rungang, Yao Shangwei. Precipitation behavior of nickel-base alloy 625 and the related factors[J]. Development and Application of Materials, 2016, 31(1): 87-91.
[15] 孟斌. 热处理对GH3625合金管材组织及性能的影响[D]. 兰州: 兰州理工大学, 2018.
Meng Bin. Effect of heat treatment on microstructure and properties of GH3625 alloy tubes[D]. Lanzhou: Lanzhou University of Technology, 2018.
[16] 高钰璧, 丁雨田, 孟斌, 等. Inconel 625合金中析出相演变研究进展[J]. 材料工程, 2020, 48(5): 13-22.
Gao Yubi, Ding Yutian, Meng Bin, et al. Research progress in evolution of precipitated phases in Inconel 625 superalloy[J]. Journal of Materials Engineering, 2020, 48(5): 13-22.

Inconel 625合金组织与性能的模拟计算与高通量试验

Computational simulation and high-throughput experiment on microstructure and properties of Inconel 625 alloy

PDF

可视化

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 15

编辑推荐

Metrics

本文评价

[1]	朱帅康, 暴嘉宁, 冯毅, 赵鑫, 蔡志辉. Fe-11Mn-2Al-2Si中锰钢的动态变形行为[J]. 金属热处理, 2025, 50(8): 30-34.
[2]	张兵, 赵鸿金, 胡玉军, 叶俊峰, 梁小霞, 旷军平. 新能源汽车用电池托盘铝合金型材的力学性能与耐蚀性[J]. 金属热处理, 2025, 50(8): 63-70.
[3]	王冰, 孙瀚, 程战, 吴元科, 钟素娟, 龙伟民, 关常勇. 激光功率对18CrNiMo渗碳钢淬火层组织与性能的影响[J]. 金属热处理, 2025, 50(8): 103-109.
[4]	费海洋, 邹乾坤, 杨永, 宋孟, 李天瑞. 冷轧压下率对Hastelloy C-276合金组织与力学性能的影响[J]. 金属热处理, 2025, 50(8): 150-156.
[5]	李浩, 李杨, 杨峰, 李云超, 王海龙, 郝蕾, 王玉慧, 许强. 均热温度对1200 MPa镀锌双相钢微观组织与力学性能的影响[J]. 金属热处理, 2025, 50(8): 225-229.
[6]	仝云奇, 李炫儒, 陈忠宇, 袁晨峪, 白峭峰. 扫描速度对50CrMnMo钢表面激光熔覆铁基涂层组织与耐磨性能的影响[J]. 金属热处理, 2025, 50(7): 10-17.
[7]	白鹭, 张小娟, 周钟平, 李睿, 朱立坚, 王军喜. 热旋压及时效处理TC11钛合金的组织与性能[J]. 金属热处理, 2025, 50(7): 61-65.
[8]	苗秉希, 康纪龙, 马志尧, 李嘉胜, 王星浩, 高明玉, 褚克, 强小虎. Al-20Si-xCu过共晶合金的固溶处理及力学性能[J]. 金属热处理, 2025, 50(7): 112-117.
[9]	李志昂, 陈晨, 赵禹栋, 王学慧, 邢鑫, 张子悦, 董奇伟. 连续退火温度对高Cr热成形钢组织与性能的影响[J]. 金属热处理, 2025, 50(7): 280-285.
[10]	陶乐晓. 纳米陶瓷颗粒对超高强铝合金组织与性能的影响[J]. 金属热处理, 2025, 50(6): 27-31.
[11]	李阳, 张威. 钒对304N奥氏体不锈钢组织与力学性能的影响[J]. 金属热处理, 2025, 50(6): 32-37.
[12]	陈瑞, 陈保安, 李梦琳, 韩钰, 祝志祥, 杨长龙, 郑维刚, 夏霏霏. 退火态铝合金导体的压缩蠕变[J]. 金属热处理, 2025, 50(6): 54-58.
[13]	解炜, 张明玉, 梁飞龙, 岳旭, 张天蔚. 包覆叠轧工艺对TC4钛合金板材组织与力学性能的影响[J]. 金属热处理, 2025, 50(6): 67-72.
[14]	赵勇, 吴裕, 刘超红, 伍晓勇, 方忠强, 强瑞. 铸态U-10wt%Zr合金的微观组织及第二相[J]. 金属热处理, 2025, 50(6): 73-78.
[15]	郭斯源, 罗巍, 徐登伟, 张腾, 宋达, 师春生. 65Si2MnWA钢螺旋压缩弹簧的应力松弛行为与组织演变[J]. 金属热处理, 2025, 50(6): 89-94.