累积叠轧对层状AX10/ZK60镁合金复合材料组织与力学性能的影响

doi:10.13251/j.issn.0254-6051.2025.07.033

金属热处理 ›› 2025, Vol. 50 ›› Issue (7): 232-240.DOI: 10.13251/j.issn.0254-6051.2025.07.033

累积叠轧对层状AX10/ZK60镁合金复合材料组织与力学性能的影响

石昊宇¹, 杨洪强², 潘军波³, 陈明¹, 张万顺^4,5,6, 罗文博⁶, 赵红阳⁵, 李昊⁵

1.辽宁科技大学机械工程与自动化学院, 辽宁鞍山 114051;
2.新昌县科创自动化设备有限公司, 浙江绍兴 312000;
3.浙江富士精工科技有限公司, 浙江绍兴 312000;
4.省部共建耐火材料与冶金国家重点实验室(武汉科技大学), 湖北武汉 430000;
5.辽宁科技大学土木工程学院, 辽宁鞍山 114051;
6.华北电力大学能源电力创新研究院, 北京 102206

收稿日期:2025-01-13 修回日期:2025-04-25 出版日期:2025-07-25 发布日期:2025-07-28
通讯作者: 李昊,讲师,硕士,E-mail:lh13904180780@163.com
作者简介:石昊宇(2000—),男,硕士研究生,主要研究方向为层状复合板材制备及性能研究,E-mail:2187159230@qq.com。
基金资助:
省部共建耐火材料与冶金国家重点实验室项目(G202408);辽宁省高校基本科研业务费专项(LJ212410146041);辽宁科技大学优秀博士基金(2023YQ05)

Effect of accumulative roll bonding on microstructure and mechanical properties of laminated AX10/ZK60 magnesium alloy composites

Shi Haoyu¹, Yang Hongqiang², Pan Junbo³, Chen Ming¹, Zhang Wanshun^4,5,6, Luo Wenbo⁶, Zhao Hongyang⁵, Li Hao⁵

1. College of Mechanical Engineering and Automation, University of Science and Technology Liaoning, Anshan Liaoning 114051, China;
2. Xinchang Kechuang Automation Equipment Co., Ltd., Shaoxing Zhejiang 312000, China;
3. Zhejiang Fuji Seiko Technology Co., Ltd., Shaoxing Zhejiang 312000, China;
4. The State Key Laboratory of Refractories and Metallurgy (Wuhan University of Science and Technology), Wuhan Hubei 430000, China;
5. School of Materials and Metallurgy, University of Science and Technology Liaoning, Anshan Liaoning 114051, China;
6. Energy and Electric Power Innovation Institute, North China Electric Power University, Beijing 102206, China

Received:2025-01-13 Revised:2025-04-25 Online:2025-07-25 Published:2025-07-28

摘要/Abstract

摘要： 采用累积叠轧(Accumulative roll bonding,ARB)制备AX10/ZK60层状异构复合材料,研究累积叠轧道次对复合材料微观组织与力学性能的影响。结果表明:随着ARB道次的增加,抗拉强度和屈服强度逐渐上升,断裂总先上升后下降,但未发生明显下降。ARB第6道次的力学性能达到最佳,抗拉强度、屈服强度和断裂总分别为274 MPa、240 MPa和13.9%。材料强度的提高归因于细晶强化和第二相强化的协同作用,断裂总的提高是层间结构界面产生背应力引起的。硬度整体呈现升高趋势,这是因为ARB过程中产生的大量位错增强了材料硬度,但第5、6道次的硬度出现波动,这是由动态再结晶效应及大量亚结构的形成导致的。

关键词: 累积叠轧, 层状复合材料, 背应力, 动态再结晶, 加工硬化

Abstract: AX10/ZK60 layered heterogeneous composites were prepared by accumulative roll bonding (ARB), and the effect of cumulative rolling passes on microstructure and mechanical properties was studied. The results show that with the increase of ARB passes, the tensile strength and yield strength increase gradually, and the elongation increases first and then decreases, but no significant decrease occurs. The mechanical properties reach the best at the 6th pass, with the tensile strength, yield strength and elongation of 274 MPa, 240 MPa and 13.9%, respectively. The increase in the strength of the material is attributed to the synergistic effect of fine-grained strengthening and secondary phase strengthening. The increase in elongation is caused by the back stress at the laminated structural interface. The overall hardness shows an increasing trend, which is due to the large number of dislocations generated in the ARB process to enhance the hardness of the material, but the hardness at the 5th and 6th passes fluctuates, which is caused by the dynamic recrystallization effect and the formation of a large number of substructures.

Key words: accumulative roll bonding, laminated composites, back stress, dynamic recrystallization, work hardening

中图分类号:

石昊宇, 杨洪强, 潘军波, 陈明, 张万顺, 罗文博, 赵红阳, 李昊. 累积叠轧对层状AX10/ZK60镁合金复合材料组织与力学性能的影响[J]. 金属热处理, 2025, 50(7): 232-240.

Shi Haoyu, Yang Hongqiang, Pan Junbo, Chen Ming, Zhang Wanshun, Luo Wenbo, Zhao Hongyang, Li Hao. Effect of accumulative roll bonding on microstructure and mechanical properties of laminated AX10/ZK60 magnesium alloy composites[J]. Heat Treatment of Metals, 2025, 50(7): 232-240.

参考文献

[1] 张士卫. 阻尼镁合金的研究与应用综述[J]. 金属世界, 2019(4): 5-11.
Zhang Shiwei. Research and application summary of damping magnesium alloys[J]. Metal World, 2019(4): 5-11.
[2] 郎强, 宋刚, 刘黎明. 坡口角度对SK7钢/AZ31B镁合金搭接接头成形和力学性能的影响[J]. 机械工程学报, 2024, 60(23): 262-269.
Lang Qiang, Song Gang, Liu Liming. Effect of groove angles on forming and mechanical properties of SK7 steel/AZ31B magnesium alloy lap joint[J]. Journal of Mechanical Engineering, 2024, 60(23): 262-269.
[3] Neh K, Ullmann M, Oswald M, et al. Twin roll casting and strip rolling of several magnesium alloys[J]. Materialstoday: Proceedings, 2015, 2(S1): 45-52.
[4] 吴铮, 李全安, 陈晓亚, 等. 机器学习在镁合金应用中的研究进展[J]. 工程科学学报, 2024, 46(10): 1797-1811.
Wu Zheng, Li Quanan, Chen Xiaoya, et al. Applications of machine learning on magnesium alloys[J]. Chinese Journal of Engineering, 2024, 46(10): 1797-1811.
[5] Wang Lijia, Zhan Sha, Ruan Yutao, et al. Influence of grain size on twinning behavior of WE43 magnesium alloy during room-temperature compression deformation[J]. Journal of Rare Earths, 2024, 42: 2285-2292.
[6] 宋要斌, 李辉, 闫金顺, 等. Mg-8Al-4Sr-1Y镁合金轧板200 ℃拉伸性能研究[J]. 热加工工艺, 2017, 46(19): 167-169.
Song Yaobin, Li Hui, Yan Jinshun, et al. Research on 200 ℃ tensile properties of rolled Mg-8Al-4Sr-1Y magnesium alloy sheet[J]. Hot Working Technology, 2017, 46(19): 167-169.
[7] Xu Y, Hu L X, Sun Y. Dynamic recrystallization kinetics of as-cast AZ91D alloy[J]. Transactions of Nonferrous Metals Society of China, 2014, 24(6): 1683-1689.
[8] 陈明, 孙贺, 赵红阳, 等. ME21稀土镁合金薄板微观组织的多尺度研究[J]. 中国科学: 技术科学, 2022, 52(10): 1571-1581.
Chen Ming, Sun He, Zhao Hongyang, et al. Multi-scale study on microstructure of ME21 rare-earth magnesium alloy sheet[J]. Scientia Sinica (Technologica), 2022, 52(10): 1571-1581.
[9] Saito Y, Ytsunomiya H, Tsuji N, et al. Novel ultra-high straining process for bulk materials—Development of the accumulative roll-bonding (ARB) process[J]. Acta Materialia, 1999, 47(2): 579-583.
[10] 郝肖杰, 聂金凤, 伍玉立, 等. 累积叠轧制备层状铝基复合材料研究进展[J]. 中国有色金属学报, 2023, 33(6): 1707-1719.
Hao Xiaojie, Nie Jinfeng, Wu Yuli, et al. Research progress of laminated aluminum matrix composites prepared by accumulative rolling bonding[J]. The Chinese Journal of Nonferrous Metals, 2023, 33(6): 1707-1719.
[11] Mo T Q, Chen Z J, Li B X, et al. Tailoring of interface structure and mechanical properties in ARBed 1100/7075 laminated composites by cold rolling[J]. Materials Science and Engineering A, 2019, 755(7): 97-105.
[12] Guo J, Sun W, Xiang N, et al. Interfacial bonding and fracture behaviors of AZ63 magnesium alloy sheet processed by accumulative roll bonding[J]. Materials, 2023, 16(14): 4981.
[13] Samiei S, Dini G, Ebrahimian-Hosseinabadi M, et al. Correlation between microstructure, mechanical properties, and corrosion characteristics of AZ31 Mg alloy processed by accumulative roll bonding process[J]. Metals and Materials International, 2023, 29(1): 192-203.
[14] Li S, Jin J, Wang Y, et al. Experimental and simulation study on mechanical properties of ZK60 magnesium alloy after accumulative roll bonding[J]. Journal of Physics: Conference Series, 2024, 2842: 012036.
[15] 陈兴章. 层状金属复合材料技术创新及发展趋势综述[J]. 有色金属材料与工程, 2017, 38(2): 63-66.
Chen Xingzhang. Review of laminar composite metal material manufacturing technique[J]. Nonferrous Metal Materials and Engineering, 2017, 38(2): 63-66.
[16] Luo Xuan, Huang Tianlin, Wang Yuhui, et al. Strong and ductile AZ31 Mg alloy with a layered bimodal structure[J]. Scientific Reports, 2019, 9(1): 5428.
[17] Wang M, Jiang X, Sun H, et al. Synergistic reinforcement of Cu/Ti₃SiC₂/C laminated-like composites with the bimodal and highly oriented graphite flake and graphene nanoplatelets[J]. Ceramics International, 2024, 50(18): 33283-33297.
[18] Li N, Chang Y, Li M, et al. Enhanced mechanical property by introducing bimodal grains structures in Cu-Ta alloys fabricated by mechanical alloying[J]. Journal of Materials Science and Technology, 2024, 172: 104-112.
[19] Mashhadi A, Atrian A, Ghalandari L, et al. Mechanical and microstructural investigation of Zn/Sn multilayered composites fabricated by accumulative roll bonding (ARB) process[J]. Journal of Alloys and Compounds, 2017, 727: 1314-1323.
[20] Zeng L F, Gao R, Fang Q F, et al. High strength and thermal stability of bulk Cu/Ta nanolamellar multilayers fabricated by cross accumulative roll bonding[J]. Acta Materialia, 2016, 110: 341-351.
[21] Du J, Li J, Feng Y, et al. Effect of layered heterogeneous microstructure design on the mechanical behavior of medium carbon steel[J]. Materials and Design, 2022, 221: 110953.
[22] Ning H, Wang C, Gao Y, et al. Understanding the deformation behaviours of Mg alloys with dispersed non-basal grain-embedded orientation heterostructures[J]. Acta Materialia, 2024, 267: 119727.
[23] 杜旭东. Mg-Al-Ca系合金凝固行为及热裂机理研究[D]. 沈阳工业大学, 2023.
[24] 杜宜卓, 郭恩宇. 挤压温度对TC4_p/ZK60复合材料组织及性能的影响[J]. 特种铸造及有色合金, 2024, 44(8): 1097-1103.
Du Yizhuo, Guo Enyu. Influence of extrusion temperature on microstructure and properties of TC4_p/ZK60 composites[J]. Special Casting and Nonferrous Alloys, 2024, 44(8): 1097-1103.
[25] 常海, 徐超, 胡小石. 累积叠轧纯Mg/ZK60镁合金层状金属复合材料的组织与性能[J]. 复合材料学报, 2019, 36(1): 178-185.
Chang Hai, Xu Chao, Hu Xiaoshi. Microstructure evolution and mechanical properties of Mg/ZK60 laminated composite fabricated by accumulated roll-bonding[J]. Acta Materiae Compositae Sinica, 2019, 36(1): 178-185.
[26] Zeng L F, Gao R, Fang Q F, et al. High strength and thermal stability of bulk Cu/Ta nanolamellar multilayers fabricated by cross accumulative roll bonding[J]. Acta Materialia, 2016, 110: 341-351.
[27] Hwang Y M, Hsu H H, Lee H J. Analysis of plastic instability during sandwich sheet rolling[J]. International Journal of Machine Tools and Manufacture, 1996, 36(1): 47-62.
[28] Ma X, Huang C, Moering J, et al. Mechanical properties of copper/bronze laminates: Role of interfaces[J]. Acta Materialia, 2016, 116: 43-52.
[29] Meng Y, Zhang H, Lin B, et al. Microstructure and mechanical properties of the AZ31/GW103K bimetal composite rods fabricated by co-extrusion[J]. Materials Science and Engineering A, 2022, 833: 142578.
[30] 唐意智, 何维均, 蒋斌. 累积叠轧Mg/Ti复合材料的微观组织与力学性能[J]. 材料热处理学报, 2023, 44(10): 59-67.
Tang Yizhi, He Weijun, Jiang Bin. Microstructure and mechanical properties of Mg/Ti laminated composites fabricated by accumulative roll bonding[J]. Transactions of Materials and Heat Treatment, 2023, 44(10): 59-67.
[31] 杨然, 宋韶杰, 刘飞龙, 等. 累积叠轧焊Cu/Nb多层材料中的滑移传递研究[J]. 金属学报, 2024-12-18.
Yang Ran, Song Shaojie, Liu Feilong, et al. Slip transfer in accumulative roll bonding Cu/Nb multilayer composites[J]. Acta Metallurgica Sinica, 2024-12-18.
[32] Alil A, PopovićM, RadetićT, et al. Influence of an accumulative roll bonding (ARB) process on the properties of AA5083 Al-Mg alloy sheets[J]. Metallurgical and Materials Engineering, 2014, 20(4): 285-95.
[33] 江鹏, 李骆宾, 张可, 等. 累积叠轧制备石墨烯/铝复合材料的组织与性能[J]. 热加工工艺, 2022, 51(22): 68-73.
Jiang Peng, Li Luobin, Zhang Ke, et al. Microstructure and properties of graphene/aluminum composites prepared by accumulative roll bonding[J]. Hot Working Technology, 2022, 51(22): 68-73.
[34] 管笛, 曲美晶, 花福安. 累积叠轧温度对AZ31镁合金组织和性能的影响[J]. 金属热处理, 2021, 46(11): 78-83.
Guan Di, Qu Meijing, Hua Fuan. Effects of accumulative roll bonding temperature on microstructure and mechanical properties of AZ31 magnesium alloy[J]. Heat Treatment of Metals, 2021, 46(11): 78-83.
[35] 贾少伟, 张郑, 王文, 等. 超细晶/纳米晶反Hall-Petch变形机制最新研究进展[J]. 材料导报, 2015, 29(23): 114-118.
Jia Shaowei, Zhang Zheng, Wang Wen, et al. The current situation of deformation mechanism on inverse Hall-Petch in crystalline material[J]. Materials Reports, 2015, 29(23): 114-118.

累积叠轧对层状AX10/ZK60镁合金复合材料组织与力学性能的影响

Effect of accumulative roll bonding on microstructure and mechanical properties of laminated AX10/ZK60 magnesium alloy composites

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