新型Co-Ni基高温合金的热变形行为及微观组织演变

doi:10.13251/j.issn.0254-6051.2024.02.001

金属热处理 ›› 2024, Vol. 49 ›› Issue (2): 1-7.DOI: 10.13251/j.issn.0254-6051.2024.02.001

• 组织与性能 • 下一篇

新型Co-Ni基高温合金的热变形行为及微观组织演变

付志强^1,2, 何国爱^1,2,3, 吴赟杰^1,2, 贺存孝^1,2

1.中南大学轻合金研究院, 湖南长沙 410083;
2.中南大学高性能复杂制造国家重点实验室, 湖南长沙 410083;
3.湖南中创空天新材料股份有限公司, 湖南岳阳 414000

收稿日期:2023-08-27 修回日期:2023-12-15 出版日期:2024-03-27 发布日期:2024-03-27
通讯作者: 何国爱,副教授,博士,E-mail:heguoai@csu.edu.cn
作者简介:付志强(1998—),男,工程师,硕士,主要研究方向为高温合金热变形,E-mail:15189103774@163.com。
基金资助:
国家自然科学基金(51901247)

Hot deformation behavior and microstructure evolution of a novel Co-Ni-based superalloy

Fu Zhiqiang^1,2, He Guoai^1,2,3, Wu Yunjie^1,2, He Cunxiao^1,2

1. Institute of Light Alloy Research, Central South University, Changsha Hunan 410083, China;
2. State Key Laboratory of High Performance Complex Manufacturing, Central South University, Changsha Hunan 410083, China;
3. Hunan InnoChina Advanced Materials Co., Ltd., Yueyang Hunan 414000, China

Received:2023-08-27 Revised:2023-12-15 Online:2024-03-27 Published:2024-03-27

摘要/Abstract

摘要： 利用Gleeble-3800热模拟试验机对新型Co-Ni基高温合金进行热压缩试验,研究其在变形温度为950~1100 ℃、应变速率为0.01~10 s^-1、真应变为0.693时的热变形行为和微观组织演变。结果表明,合金流动应力随变形温度的升高或应变速率的降低而减小。合金平均晶粒尺寸随变形温度的升高而增加,降低变形温度和提高应变速率可细化动态再结晶晶粒。基于EBSD和TEM分析表明,合金热变形过程中非连续动态再结晶(DDRX)作为主要动态再结晶(DRX)机制,孪晶形核作为辅助形核机制。

关键词: Co-Ni基高温合金, 热压缩, 动态再结晶, 孪晶

Abstract: Gleeble-3800 thermal simulation testing machine was used to perform hot compression tests on a novel Co-Ni-based superalloy to study its hot deformation behavior and microstructure evolution at deformation temperature of 950-1100 ℃, strain rate of 0.01-10 s^-1 and true strain of 0.693. The results show that the flow stress of the alloy decreases with the increase of deformation temperature or the decrease of strain rate. The average grain size of the alloy increases with the increase of deformation temperature and the dynamic recrystallization grains can be refined by reducing the deformation temperature and increasing the strain rate. The EBSD and TEM analysis results indicate that the discontinuous dynamic recrystallization (DDRX) is the main dynamic recrystallization (DRX) mechanism and the twin nucleation is the auxiliary nucleation mechanism during the hot deformation of the alloy.

Key words: Co-Ni-based superalloy, hot compression, dynamic recrystallization, twin

中图分类号:

TG146.1

付志强, 何国爱, 吴赟杰, 贺存孝. 新型Co-Ni基高温合金的热变形行为及微观组织演变[J]. 金属热处理, 2024, 49(2): 1-7.

Fu Zhiqiang, He Guoai, Wu Yunjie, He Cunxiao. Hot deformation behavior and microstructure evolution of a novel Co-Ni-based superalloy[J]. Heat Treatment of Metals, 2024, 49(2): 1-7.

参考文献

[1]Lu S, Shang B, Luo Z, et al. Investigation on the cold deformation strengthening mechanism in MP159 alloy[J]. Metallurgical and Materials Transactions A, 2000, 31(1): 5-13.
[2]Gu J, Guo L, Gan B, et al. Microstructure and mechanical properties of an MP159 alloy processed by torsional deformation and subsequent annealing[J]. Materials Science and Engineering: A, 2021, 802: 140676.
[3]Zhang W W, Yang Y, Tan Y B, et al. Microstructure evolution and strengthening mechanisms of MP159 superalloy during room temperature rolling and cryorolling[J]. Journal of Alloys and Compounds, 2022, 908: 164667.
[4]黄钲钦, 王岩, 刘敏学, 等. 变形参数对FGH96合金热机械处理组织与性能的影响[J]. 中国有色金属学报, 2021, 31(7): 1842-1855.
Huang Zhengqin, Wang Yan, Liu Minxue, et al. Effect of deformation parameters on microstructure and properties of thermo-mechanical treatment for FGH96 alloy[J]. The Chinese Journal of Nonferrous Metals, 2021, 31(7): 1842-1855.
[5]Yang Q, Lin Y, Chen M, et al. Modeling dynamic recrystallization behavior in a novel HIPed P/M superalloy during high-temperature deformation[J]. Materials, 2022, 15(11): 4030.
[6]Wang K, Wen D, Li J, et al. Hot deformation behaviors of low-alloyed ultrahigh strength steel 30CrMnSiNi2A: Microstructure evolution and constitutive modeling[J]. Materials Today Communications, 2021, 26: 102009.
[7]Yang Q, Lin Y, Guo J, et al. Spheroidization and dynamic recrystallization mechanisms of a novel HIPed P/M superalloy during hot deformation[J]. Journal of Alloys and Compounds, 2022, 910: 164909.
[8]Yao Z, Wang H, Dong J, et al. Characterization of hot deformation behavior and dislocation structure evolution of an advanced nickel-based superalloy[J]. Metals, 2020, 10(7): 920.
[9]Xiong J, He J, Leng X, et al. Gaussian process regressions on hot deformation behaviors of FGH98 nickel-based powder superalloy[J]. Journal of Materials Science & Technology, 2023, 146: 177-185.
[10]Song Y, Li Y, Li H, et al. Hot deformation and recrystallization behavior of a new nickel-base superalloy for ultra-supercritical applications[J]. Journal of Materials Research and Technology, 2022, 19: 4308-4324.
[11]Li H, Yang L, Wang Y, et al. Thermal deformation and dynamic recrystallization of a novel HEXed P/M nickel-based superalloy[J]. Materials Characterization, 2020, 163: 110285.
[12]Xie B, Yu H, Sheng T, et al. DDRX and CDRX of an as-cast nickel-based superalloy during hot compression at γ′ sub-/super-solvus temperatures[J]. Journal of Alloys and Compounds, 2019, 803: 16-29.
[13]Jia D, Sun W, Xu D, et al. Dynamic recrystallization behavior of GH4169G alloy during hot compressive deformation[J]. Journal of Materials Science & Technology, 2019, 35(9): 1851-1859.
[14]Liu P, Zhang R, Yuan Y, et al. Microstructural evolution of a Ni-Co based superalloy during hot compression at γ′ sub-/super-solvus temperatures[J]. Journal of Materials Science & Technology, 2021, 77: 66-81.
[15]Azarbarmas M, Aghaie-Khafri M, Cabrera J M, et al. Dynamic recrystallization mechanisms and twining evolution during hot deformation of Inconel 718[J]. Materials Science and Engineering: A, 2016, 678: 137-152.
[16]Du B N, Hu Z Y, Sheng L Y, et al. Microstructural characteristics and mechanical properties of the hot extruded Mg-Zn-Y-Nd alloys[J]. Journal of Materials Science & Technology, 2021, 60: 44-55.

新型Co-Ni基高温合金的热变形行为及微观组织演变

Hot deformation behavior and microstructure evolution of a novel Co-Ni-based superalloy

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