金属热处理 ›› 2025, Vol. 50 ›› Issue (12): 166-170.DOI: 10.13251/j.issn.0254-6051.2025.12.025

• 工艺研究 • 上一篇    下一篇

正火对16Cr3NiWMoVNbE钢棒材边缘处粗晶的影响

孙勇, 庞学东, 翟羽佳, 温博, 信振飞, 梁晓东, 郭子鹤   

  1. 抚顺特殊钢股份有限公司 技术中心, 辽宁 抚顺 113000
  • 收稿日期:2025-08-14 修回日期:2025-10-21 发布日期:2026-01-06
  • 作者简介:孙 勇(1985—),男,高级工程师,学士,主要研究方向为超高强度齿轮轴承钢、航空用钢等研发和生产,E-mail:sysyong@163.com

Effect of normalizing on coarse crystal at edge of 16Cr3NiWMoVNbE steel bar

Sun Yong, Pang Xuedong, Zhai Yujia, Wen Bo, Xin Zhenfei, Liang Xiaodong, Guo Zihe   

  1. Technology Center, Fushun Special Steel Co., Ltd., Fushun Liaoning 113000, China
  • Received:2025-08-14 Revised:2025-10-21 Published:2026-01-06

摘要: 采用OM、SEM等研究了正火处理(940/1000 ℃×120 min空冷)对高强度16Cr3NiWMoVNbE钢棒材边缘处粗晶的影响。结果表明,1000 ℃正火处理对棒材边缘粗晶有显著的晶粒细化作用,晶粒细化到7级;940 ℃正火处理对棒材边缘粗晶有一定的改善作用,但粗晶区域未能完全消除,原因在于原奥氏体晶界附近及基体大量M(C, N)类碳化物未能完全溶解,阻碍了静态再结晶。此外,粗晶产生的原因为锻造末火次成材时棒材的表面层降温较快,热力学上不能满足晶粒迁移及长大,影响再结晶过程,钢棒边缘处于两相区热变形临界条件,导致少量铁素体沿晶界形成块状组织,进而在检验试片上检验显示粗晶。

关键词: 航空齿轮材料, 16Cr3NiWMoVNbE钢, 边缘粗晶, 正火处理, 锻造温度

Abstract: Effect of normalizing treatment (940/1000 ℃×120 min, air cooling) on the coarse grains at the edge of high-strength 16Cr3NiWMoVNbE steel bars were investigated by means of OM and SEM. The results show that normalizing at 1000 ℃ has a significant refinement effect on the coarse grains at the edge of the steel bars, with the grains refining to grade 7. Normalizing at 940 ℃ has a certain improvement effect on the coarse grains at the edge of the steel bars, but the coarse grain area cannot be completely eliminated. The reason is that a large amount of M(C, N) type carbides near the original austenite grain boundaries and in the matrix cannot be completely dissolved, which hinders static recrystallization. In addition, the reason for the formation of coarse grains is that the surface layer of the steel bars cools down faster during the last forging pass, and thermodynamically it cannot meet the requirements of grain migration and growth, which affects the recrystallization process. The edge of the steel bars is in a critical condition of two-phase zone hot deformation, resulting in a small amount of ferrite forming blocky structures along the grain boundaries, which is displayed as coarse grains on the inspection specimens.

Key words: aviation gear material, 16Cr3NiWMoVNbE steel, coarse crystal at the edge, normalizing treatment, forging temperature

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