金属热处理 ›› 2025, Vol. 50 ›› Issue (12): 89-95.DOI: 10.13251/j.issn.0254-6051.2025.12.014

• 工艺研究 • 上一篇    下一篇

退火温度对含铜TWIP钢微观组织与力学性能的影响

郭振龙1, 白玉1,2, 丁震1, 韩毓瑶1, 于巍1, 郝海1,2   

  1. 1.大连理工大学 材料科学与工程学院 辽宁省凝固控制与数字化制备技术重点实验室, 辽宁 大连 116024;
    2.大连理工大学 宁波研究院, 浙江 宁波 315018
  • 收稿日期:2025-07-25 修回日期:2025-10-20 发布日期:2026-01-06
  • 通讯作者: 白 玉,副教授,博士,E-mail:ybai@dlut.edu.cn
  • 作者简介:郭振龙(2001—),男,博士研究生,主要研究方向为TWIP钢强韧化和变形机制,E-mail:18939646760@163.com。
  • 基金资助:
    国家自然科学基金青年项目(52201110);宁波市重点研发计划(2022Z048)

Effect of annealing temperature on microstructure and mechanical properties of TWIP steels containing copper

Guo Zhenlong1, Bai Yu1,2, Ding Zhen1, Han Yuyao1, Yu Wei1, Hao Hai1,2   

  1. 1. Key Laboratory of Solidification Control and Digital Preparation Technology (Liaoning Province), School of Materials Science and Engineering, Dalian University of Technology, Dalian Liaoning 116024, China;
    2. Ningbo Research Institute, Dalian University of Technology, Ningbo Zhejiang 315018, China
  • Received:2025-07-25 Revised:2025-10-20 Published:2026-01-06

摘要: 采用电子背散射衍射(EBSD)、X射线衍射(XRD)、扫描电镜(SEM)以及力学性能测试等手段,研究了退火温度对含铜TWIP钢微观组织与力学性能的影响。通过热力学模型的计算,Fe-22Mn-0.6C-3Cu TWIP钢在室温下的层错能为27.95 mJ/m2,其变形机制以孪生为主。结果显示,随着退火温度的降低,含Cu TWIP钢的微观组织从均匀粗大的等轴晶逐渐向细晶和超细晶混合组织转变,屈服强度和抗拉强度升高,断后伸长率下降;随着平均晶粒尺寸的减小,动态应变时效现象会推迟发生。通过多道次冷轧和低温短时退火(650 ℃×5 min)制备的超细晶(Ultrafine grain,UFG)含Cu TWIP钢表现出最优的力学性能,其屈服强度为643 MPa,抗拉强度为1104 MPa,伸长率为78.5%,强塑积为86.4 GPa·%。

关键词: TWIP钢, 退火温度, 超细晶, 屈服强度, 强塑积

Abstract: Effect of annealing temperature on the microstructure and mechanical properties of Cu-containing TWIP steel was studied using electron backscatter diffraction(EBSD), X-ray diffraction(XRD), scanning electron microscope(SEM), and mechanical testing. Thermodynamic calculations reveal that the stacking fault energy (SFE) of Fe-22Mn-0.6C-3Cu TWIP steel at room temperature is 27.95 mJ/m2, indicating that the deformation is primarily dominated by twinning. The results show that as the annealing temperature decreases, the microstructure of the Cu-containing TWIP steel evolves from homogeneous coarse equiaxed grain to mixed microstructure of fine and ultrafine grains. Correspondingly, the yield strength and tensile strength increase, while the elongation decreases. Moreover, as the average grain size decreases, the onset of dynamic strain aging is delayed. The ultrafine-grained (UFG) Cu-containing TWIP steel, fabricated through multi-pass cold rolling followed by low-temperature short-time annealing (650 ℃×5 min), exhibits the optimal mechanical properties. The steel achieves a yield strength of 643 MPa, a tensile strength of 1104 MPa, an elongation of 78.5%, and a product of tensile strength and elongation of 86.4 GPa·%.

Key words: twinning induced plasticity(TWIP) steel, annealing temperature, ultrafine grain, yield strength, product of tensile strength and elongation

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