气雾化参数对SLM用1720 MPa级马氏体时效钢粉末特性的影响

doi:10.13251/j.issn.0254-6051.2022.09.010

金属热处理 ›› 2022, Vol. 47 ›› Issue (9): 54-59.DOI: 10.13251/j.issn.0254-6051.2022.09.010

气雾化参数对SLM用1720 MPa级马氏体时效钢粉末特性的影响

刘再西^1,2, 卢德宏¹, 王长军², 刘振宝², 梁剑雄²

1.昆明理工大学材料科学与工程学院, 云南昆明 650032;
2.钢铁研究总院特殊钢研究院, 北京 100089

收稿日期:2022-04-12 修回日期:2022-07-13 发布日期:2022-10-18
通讯作者: 卢德宏,教授,博士,E-mail: ldhongkust@126.com
作者简介:刘再西(1995—),男,硕士研究生,主要研究方向为马氏体钢热处理,E-mail:962314414@qq.com。

Effect of gas atomization parameters on characteristics of 1720 MPa maraging steel powder used for selective laser melting process

Liu Zaixi^1,2, Lu Dehong¹, Wang Changjun², Liu Zhenbao², Liang Jianxiong²

1. School of Materials Science and Engineering, Kunming University of Science and Technology, Kunming Yunnan 650032, China;
2. Special Steel Research Institute, Central Iron and Steel Research Institute, Beijing 100089, China

Received:2022-04-12 Revised:2022-07-13 Published:2022-10-18

摘要/Abstract

摘要： 利用真空感应熔炼气雾化法制备1720 MPa级马氏体时效钢粉末,研究雾化压力、过热度、气体加热温度对粉末特性的影响。结果表明,当雾化压力较高、过热度较高、气体加热温度较高的情况下,金属粉末的细粉收得率较大,松装密度较高,流动性较好。最佳雾化参数为漏嘴孔径ϕ5 mm、雾化压力5.0 MPa、过热度245 K、雾化气体温度100 ℃。该工艺条件下的时效钢粉末球形度良好,粉末流动性为20.15 s/50 g,松装密度为4.23 g/cm。

关键词: 马氏体时效钢, 气雾化, 过热度, 金属粉末

Abstract: 1720 MPa maraging steel powders were manufactured by vacuum induction melting gas atomization (VIGA) process, and the effect of atomization pressure, superheat degree and gas heating temperature on powder characteristics was studied. The results show that when the atomization pressure, superheat degree and gas heating temperature are relatively higher, the yield of fine metal powder and the bulk density are higher, and the powder flowability is better. The optimal atomization parameters are the nozzle diameter of ϕ5 mm, the atomization pressure of 5.0 MPa, the superheat degree of 245 K, and the gas atomization temperature of 100 ℃. The aging steel powder under this process has good sphericity with powder flowability of 20.15 s/50 g and bulk density of 4.23 g/cm³.

Key words: maraging steel, gas atomization, superheat, metal powder

中图分类号:

TG143.1

刘再西, 卢德宏, 王长军, 刘振宝, 梁剑雄. 气雾化参数对SLM用1720 MPa级马氏体时效钢粉末特性的影响[J]. 金属热处理, 2022, 47(9): 54-59.

Liu Zaixi, Lu Dehong, Wang Changjun, Liu Zhenbao, Liang Jianxiong. Effect of gas atomization parameters on characteristics of 1720 MPa maraging steel powder used for selective laser melting process[J]. Heat Treatment of Metals, 2022, 47(9): 54-59.

参考文献

[1]Gu D, Shi X, Poprawe R, et al. Material-structure-performance integrated laser-metal additive manufacturing[J]. Science, 2021, 372(6545): 1-16.
[2]Liu G, Zhang X, Chen X, et al. Additive manufacturing of structural materials[J]. Materials Science and Engineering R: Reports, 2021, 145: 100596.
[3]谭超林, 周克崧, 马文有, 等. 激光增材制造成型马氏体时效钢研究进展[J]. 金属学报, 2020, 56(1): 36-52.
Tan Chaolin, Zhou Kesong, Ma Wenyou, et al. Research progress of laser additive manufacturing of maraging steels[J]. Acta Metallurgica Sinica, 2020, 56(1): 36-52.
[4]时雨, 卫广智, 赵飞. 18Ni(1720 MPa)型马氏体时效钢时效工艺研究[J]. 兵器材料科学与工程, 2013(3): 89-91.
Shi Yu, Wei Guangzhi, Zhao Fei. Aging process of 18Ni(1720 MPa) maraging steel[J]. Ordnance Material Science and Engineering, 2013(3): 89-91.
[5]康凯. 选区激光成形用18Ni-300粉末特性及成形件组织结构的研究[D]. 重庆: 重庆大学, 2014.
[6]Król M, Snopiński P, Czech A. The phase transitions in selective laser-melted 18-Ni(300-grade) maraging steel[J]. Journal of Thermal Analysis and Calorimetry, 2020, 142(2): 1011-1018.
[7]Zhang H, Sun M, Liu Y, et al. Ultrafine-grained dual-phase maraging steel with high strength and excellent cryogenic toughness[J]. Acta Materialia, 2021, 211: 116878.
[8]沈英俊, 季道馨, 徐永利, 等. 若干雾化参数的理论简析[J]. 粉末冶金技术, 1995(1): 21-25.
Shen Yingjun, Ji Daoxin, Xu Yongli, et al. Brief theoretical analyses on some atomising parameters[J]. Powder Metallurgy Technology, 1995(1): 21-25.
[9]李鑫, 王永祥. 气雾化工艺参数对金属粉末粒度影响的研究[J]. 江西有色金属, 2002, 16(3): 27-29.
Li Xin, Wang Yongxiang. Study on the effect of atomization parameters on the granularity of metal powder[J]. Jiangxi Nonferrous Metals, 2002, 16(3): 27-29.
[10]朱晓飞, 周舸, 李正元, 等. 气雾化参数对304不锈钢3D打印专用粉末粒径的影响[J]. 沈阳工业大学学报, 2021, 43(6): 646-651.
Zhu Xiaofei, Zhou Ge, Li Zhengyuan, et al. Effect of atomization parameters on particle size of 304 stainless steel powders exclusively for 3D printing[J]. Journal of Shenyang University of Technology, 2021, 43(6): 646-651.
[11]张梦醒, 王长军, 陈清明, 等. 气雾化参数对PH13-8Mo钢粉末特性的影响[J]. 金属热处理, 2019, 44(12): 112-115.
Zhang Mengxing, Wang Changjun, Chen Qingming, et al. Effects of processing parameters of gas atomization on characteristics of PH13-8Mo steel powders[J]. Heat Treatment of Metals, 2019, 44(12): 112-115.
[12]王长军, 张梦醒, 陈清明, 等. 真空感应熔炼气雾化法制备高强度PH13-8Mo钢粉末的特性表征[J]. 材料热处理学报, 2020, 41(1): 94-101.
Wang Changjun, Zhang Mengxing, Chen Qingming, et al. Characterization of high strength PH13-8Mo steel powders prepared by vacuum induction melting gas atomization method[J]. Transactions of Materials and Heat Treatment, 2020, 41(1): 94-101.
[13]郭景杰, 傅恒志. 合金熔体及其处理[M]. 北京: 机械工业出版社, 2005.
Guo Jingjie, Fu Hengzhi. Alloy Melt and Its Treatment[M]. Beijing: China Machine Press, 2005.
[14]Sarkar S B, Ray H S. Analysis of kinetic data by Johnson-Mehl equation[J]. Journal of Thermal Analysis, 1990, 36(1): 231-242.
[15]Nichiporenko O S, Naida Y I. Heat exchange between metal particles and gas in the atomization process[J]. Soviet Powder Metallurgy and Metal Ceramics, 1968, 7(7): 509-512.

气雾化参数对SLM用1720 MPa级马氏体时效钢粉末特性的影响

Effect of gas atomization parameters on characteristics of 1720 MPa maraging steel powder used for selective laser melting process

PDF

可视化

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 6

编辑推荐

Metrics

本文评价

[1]	董福元, 张明旭, 侯俊峰. 时效时间对SLM 18Ni300马氏体时效钢组织性能的影响[J]. 金属热处理, 2021, 46(6): 88-91.
[2]	马聪慧, 王长军, 沈韬, 胡家齐, 梁剑雄. VIGA法制备的M2052锰铜合金粉末及其SLM打印件的性能[J]. 金属热处理, 2020, 45(10): 140-147.
[3]	姚春臣1，王海云1，刘宪民2，王春旭2. 无Co马氏体时效钢筒形锻件的晶粒细化[J]. 金属热处理, 2016, 41(2): 140-142.
[4]	厉鑫洋，厉勇，刘宪民，黄顺喆，王春旭，罗文英. 时效温度对18Ni(250)马氏体时效钢低周疲劳性能的影响[J]. 金属热处理, 2015, 40(4): 69-73.
[5]	门蒙蒙，杨卓越，丁雅莉，宁静. 时效温度对18Ni350马氏体时效钢缺口效应和延迟断裂的影响[J]. 金属热处理, 2015, 40(10): 162-165.
[6]	张占玲, 赵飞, 时雨. 多层次细化对18Ni马氏体时效钢断裂韧性的影响[J]. 金属热处理, 2014, 39(8): 74-77.