金属热处理 ›› 2022, Vol. 47 ›› Issue (8): 188-193.DOI: 10.13251/j.issn.0254-6051.2022.08.032

• 工艺研究 • 上一篇    下一篇

热处理对DZ125定向凝固合金组织结构与蠕变行为的影响

田宁1,2, 赵国旗1,2, 张萍1, 向贤礼1, 田素贵1, 张顺科1,2, 闫化锦1   

  1. 1.贵州工程应用技术学院 机械学院, 贵州 毕节 551700;
    2.沈阳工业大学 材料科学与工程学院, 辽宁 沈阳 110870
  • 收稿日期:2022-05-07 修回日期:2022-07-03 出版日期:2022-08-25 发布日期:2022-09-19
  • 通讯作者: 赵国旗,副教授,博士,E-mail:zhaoguoqi1986@163.com
  • 作者简介:田 宁(1984—),男,副教授,博士,主要研究方向为材料的组织与性能控制,E-mail:Syhgxytn@163.com。
  • 基金资助:
    贵州省科学技术基金(20201Y198);毕节市科学技术项目(20192);贵州省教育厅青年科技人才成长计划([2022]121);贵州省科技计划([2019]2843);毕节市科技局贵州工程应用技术学院联合基金(G[2022]21, G[2022]22)

Effect of heat treatment on microstructure and creep behavior of directionally solidified alloy DZ125

Tian Ning1,2, Zhao Guoqi1,2, Zhang Ping1, Xiang Xianli1, Tian Sugui1, Zhang Shunke1,2, Yan Huajin1   

  1. 1. School of Mechanical Engineering, Guizhou University of Engineering Science, Bijie Guizhou 551700, China;
    2. School of Materials Science and Engineering, Shenyang University of Technology, Shenyang Liaoning 110870, China
  • Received:2022-05-07 Revised:2022-07-03 Online:2022-08-25 Published:2022-09-19

摘要: 通过不同条件蠕变性能测试及组织形貌观察,研究了热处理对DZ125合金的组织结构演变和蠕变行为的影响规律。结果表明,铸态合金的枝晶间区域存在较多放射状的共晶组织,在枝晶间和枝晶干处部分γ′相呈蝶形形态且γ′相尺寸具有较大差异。铸态合金的共晶组织及γ′相在固溶过程中被溶解,并在随后的冷却过程中类菱形的细小γ′相自γ基体中析出;一次时效期间,类菱形的细小γ′相发生钝化并长大直至转变成立方体形态;二次时效期间,γ′相的尺寸基本不变,但立方度增加,合金的组织结构为γ′相以共格方式自γ基体中析出。在热处理过程中基本消除了合金中的共晶组织,并提高了γ′相的立方度,但并未消除合金中的组织不均匀性,枝晶干区域的立方γ′相尺寸细小,而枝晶间区域的立方γ′相尺寸粗大,并且合金在980 ℃具有良好的抗蠕变性能。

关键词: DZ125镍基合金, 热处理, 组织结构, 蠕变性能

Abstract: Through creep property test and microstructure observation, the effect of heat treatment on microstructure and creep behavior of directionally solidified alloy DZ125 was studied. The results show that there are many radial eutectic structures in the interdendritic region of the as-cast alloy, and part of the γ′ phases between dendrites and dendrite stems are butterfly shaped, and the sizes of γ′ phase are quite different. The eutectic structures and γ′ phases of the as-cast alloy are dissolved during the solid solution process, and the fine rhombohedral γ′ phase precipitated from the matrix during the subsequent cooling process. During the first aging period, the small γ′ phases similar to rhombus are blunted and grown until it transformed into a cube shape. During the secondary aging, the size of the γ′ phase is basically unchanged, but the cubic degree increases, and the microstructure of the alloy is that the γ′ phase precipitated from the matrix in a coherent manner. During the heat treatment process, the eutectic structures in the alloy are basically eliminated and the cubic degree of the phase is improved, but the structure inhomogeneity in the alloy is not eliminated. The cubic γ′ phase in the dendrite stem region is small in size, while the cubic γ′ phase in the interdendritic region is coarse in size, and the alloy has good anti-creep properties at 980 ℃.

Key words: DZ125 nickel-based superalloy, heat treatment, microstructure, creep properties

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