深冷处理对TC4钛合金表面性能的影响

doi:10.13251/j.issn.0254-6051.2022.02.033

金属热处理 ›› 2022, Vol. 47 ›› Issue (2): 183-187.DOI: 10.13251/j.issn.0254-6051.2022.02.033

深冷处理对TC4钛合金表面性能的影响

师佑杰^1,2, 李永刚^1,2,3, 李文辉^1,2, 王兴富^1,2

1.太原理工大学机械与运载工程学院, 山西太原 030024;
2.精密加工山西省重点实验室, 山西太原 030024;
3.山西省金属材料腐蚀与防护工程技术研究中心, 山西太原 030024

收稿日期:2021-09-28 修回日期:2021-12-19 出版日期:2022-02-25 发布日期:2022-04-01
通讯作者: 李永刚,副教授,E-mail:liyonggang_tyut@126.com
作者简介:师佑杰(1994—),男,硕士研究生,主要研究方向为精密零件表面光整加工,E-mail:898329326@qq.com。
基金资助:
国家自然科学基金(51705352);中国博士后科学基金(2018M641682);山西省高等学校科技创新项目(2019L0139)

Effect of cryogenic treatment on surface properties of TC4 titanium alloy

Shi Youjie^1,2, Li Yonggang^1,2,3, Li Wenhui^1,2, Wang Xingfu^1,2

1. College of Mechanical and Vehicle Engineering, Taiyuan University of Technology, Taiyuan Shanxi 030024, China;
2. Shanxi Key Laboratory of Precision Processing, Taiyuan Shanxi 030024, China;
3. Engineering and Technology Research Center for Metal Material Corrosion and Protection of Shanxi Province, Taiyuan Shanxi 030024, China

Received:2021-09-28 Revised:2021-12-19 Online:2022-02-25 Published:2022-04-01

摘要/Abstract

摘要： 研究了深冷处理对TC4钛合金滚磨光整加工和表面性能的影响。对TC4钛合金试样进行深冷处理,将不同深冷时间下的试样进行滚磨光整加工,根据表面粗糙度确定适合的深冷时间后,对比分析深冷处理前后合金试样的显微组织、显微硬度及残余应力的变化。利用扫描电镜探究了深冷处理和滚磨光整加工后合金试样表面形貌的变化。结果表明,深冷处理12 h后试样表面粗糙度最小,试样组织受到冷缩内应力的作用,α相的比例从未深冷处理的56.45%增加到85.42%,组织变得均匀且致密。试样的显微硬度在深冷处理12 h时最大,比未处理试样提高了3.47%。深冷处理12 h和滚磨光整加工后的试样相比未处理试样表面残余压应力增加26.26%。粗糙度测量和扫描电镜结果显示深冷处理使钛合金试样的可加工性增强,深冷处理12 h的试样经过离心式滚磨光整加工表面粗糙度可从约0.500 μm下降到约0.250 μm,表面质量明显变好。

关键词: TC4钛合金, 深冷处理, 显微组织, 显微硬度, 残余应力, 表面粗糙度

Abstract: Effect of cryogenic treatment on barrel polishing and finishing and surface properties of the TC4 titanium alloy was studied. The TC4 titanium alloy specimen was subjected to cryogenic treatment, and the specimens under different cryogenic time were barrel polished and finished. After determining the appropriate cryogenic time according to the surface roughness, the changes of microstructure, microhardness and residual stress of the alloy specimens before and after cryogenic treatment were compared and analyzed. The change of surface morphology of the alloy after cryogenic treatment and barrel polishing and finishing was investigated by means of scanning electron microscope. The results show that the surface roughness of the specimen is the smallest after cryogenic treatment for 12 h, and the structure is affected by the internal stress of cold shrinkage, so that the proportion of α phase rises from 56.45%(untreated) to 85.42%, and the structure becomes uniform and dense. The microhardness of the alloy is the highest when cryogenic treated for 12 h, which is increased by 3.47% compared with untreated specimen. The surface residual compressive stress of the specimen increases by 26.26% after cryogenic treatment for 12 h and barrel polishing and finishing, compared with untreated specimen. Roughness measurement and scanning electron microscope results show that cryogenic treatment enhances the machinability of the titanium alloy specimen. The surface roughness of the specimen cryogenic treated for 12 h can reduce from about 0.500 μm(untreated specimen) to about 0.250 μm after barrel polishing and finishing, and the surface quality is significantly improved.

Key words: TC4 titanium alloy, cryogenic treatment, microstructure, microhardness, residual stress, surface roughness

中图分类号:

TG156.91

师佑杰, 李永刚, 李文辉, 王兴富. 深冷处理对TC4钛合金表面性能的影响[J]. 金属热处理, 2022, 47(2): 183-187.

Shi Youjie, Li Yonggang, Li Wenhui, Wang Xingfu. Effect of cryogenic treatment on surface properties of TC4 titanium alloy[J]. Heat Treatment of Metals, 2022, 47(2): 183-187.

参考文献

[1]刘广斌. 深冷处理对7050铝合金时效硬化及耐蚀性能的影响[D]. 烟台: 烟台大学, 2019.
Liu Guangbin. Effect of cryogenic treatment on precipitation hardening and corrosion resistance of 7050 aluminum alloy[D]. Yantan: Yantai University, 2019.
[2]杨永雷. 基于深冷处理的钻头磨损规律及其寿命研究[D]. 北京: 北方工业大学, 2008.
Yang Yonglei. Study on wear regularity and life of the drill based on cryogenic treatment[D]. Beijing: North China University of Technology, 2008.
[3]李树侠, 朴松花. 钛合金处理的机械加工工艺综述[J]. 飞航导弹, 2007(7): 57-61.
Li Shuxia, Pu Songhua. Overview of matching process of titanium alloy materials[J]. Aerodynamic Missile Journal, 2007(7): 57-61.
[4]李秀红, 李文辉, 王程伟, 等. TC4钛合金滚磨光整加工的表面完整性与抗疲劳性能[J]. 中国表面工程, 2018, 31(1): 15-25.
Li Xiuhong, Li Wenhui, Wang Chengwei, et al. Surface integrity and anti-fatigue performance of TC4 titanium alloy by mess finishing[J]. China Surface Engineering, 2018, 31(1): 15-25.
[5]张忠杰. 深冷处理对Ti-6A1-4V钛合金摩擦磨损行为及机理的影响[D]. 太原: 太原理工大学, 2019.
Zhang Zhongjie. The influence of cryogenic treatment on the wear behavior and mechanism of Ti-6Al-4V titanium alloy[D]. Taiyuan: Taiyuan University of Technology, 2019.
[6]雷达, 李永刚, 李文辉, 等. 深冷处理对钛合金力学性能及摩擦磨损性能的影响[J/OL]. 机械科学与技术, 2021, 40(4): 566-571.
Lei Da, Li Yonggang, Li Wenhui, et al. Study on mechanical properties and wear resistance of titanium alloys before and after cryogenic treatment[J/OL]. Mechanical Science and Technology for Aerospace Engineering, 2021, 40(4): 566-571.
[7]Öteyaka M Ö, Çakir F H, Çelik O N. Influence of shallow and deep cryogenic treatment on the corrosion behavior of Ti6Al4V alloy in isotonic solution[J]. Materials and Corrosion, 2020, 71(7): 1206-1215.
[8]陈劲松. 工业纯钛及TC4钛合金的深冷处理研究[D]. 长沙: 湖南大学, 2011.
Chen Jinsong. Effect of cryogenic treatment on industrial titanium and TC4 alloy[D]. Changsha: Hunan University, 2011.
[9]Li G R, Qin T, Fei A G, et al. Performance and microstructure of TC4 titanium alloy subjected to deep cryogenic treatment and magnetic field[J]. Journal of Alloys and Compounds, 2019, 802: 50-69.
[10]陈振华, 谢配孺, 姜勇, 等. 钛合金深冷及冷-热循环处理研究[J]. 湖南大学学报(自然科学版), 2014, 41(7): 1-5.
Chen Zhenhua, Xie Peiru, Jiang Yong, et al. Study on the perform improvement of titanium alloy through deep cryogenic and thermal-cold cycling treatment[J]. Journal of Hunan University(Natural Sciences), 2014, 41(7): 1-5.
[11]帅歌旺, 张萌. 铜合金中金相组织特征参数的测量[J]. 南昌大学学报(理科版), 2004(3): 278-280, 284.
Shuai Gewang, Zhang Meng. Measurement of characteristic parameters of metallographic structure in copper alloy[J]. Journal of Nanchang University(Natural Science), 2004(3): 278-280, 284.
[12]曾卫东, 王凯旋, 赵永庆, 等. (α+β)两相钛合金显微组织的定量分析和表征[J]. 中国有色金属学报, 2010, 20(S1): 505-509.
Zeng Weidong, Wang Kaixuan, Zhao Yongqing, et al. Quantification of microstructural features in (α+β) titanium alloys[J].The Chinese Journal of Nonferrous Metals, 2010, 20(S1): 505-509.
[13]费爱庚. 磁场深冷处理TC4钛合金的微观组织和力学性能的研究[D]. 镇江: 江苏大学, 2018.
Fei Aigeng. Research on microstructure and mechanical properties of TC4 titanium alloy subjected to the magnetic field and deep cryogenic treatment[D]. Zhenjiang: Jiangsu University, 2018.
[14]Xu L Y, Zhu J, Jing H Y, et al. Effects of deep cryogenic treatment on the residual stress and mechanical properties of electron-beam-welded Ti-6Al-4V joints[J]. Materials Science and Engineering: A, 2016, 673: 503-510.
[15]赵卫军. 深冷处理工艺对材料残余应力影响的研究[D]. 太原: 太原科技大学, 2018.
Zhao Weijun. Research on the effect of cryogenic treatment process on residual stress[D]. Taiyuan: Taiyuan University of Science and Technology, 2018.
[16]Li Y, Wang X, Yang S, et al. Investigation on wear behavior of cryogenically treated Ti-6Al-4V titanium alloy under dry and wet conditions[J]. Materials, 2019, 12(18): 2850.
[17]王兰. 钛合金磨损行为及磨损机理的研究[D]. 镇江: 江苏大学, 2014.
Wang Lan. Research on wear behavior and wear mechanism of titanium alloys[D]. Zhenjiang: Jiangsu University, 2014.

深冷处理对TC4钛合金表面性能的影响

Effect of cryogenic treatment on surface properties of TC4 titanium alloy

PDF

可视化

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 15

编辑推荐

Metrics

本文评价

[1]	张子延, 陈君, 陈晓亚, 李全安, 刘建鑫. 固溶时效处理对Mg-4Sm-3Gd-0.5Zr合金显微组织和耐蚀性能的影响[J]. 金属热处理, 2022, 47(4): 10-16.
[2]	梁恩溥, 徐乐, 杨勇, 王毛球. 添加Al、Cu对40CrNi3MoV钢组织和力学性能的影响[J]. 金属热处理, 2022, 47(4): 17-23.
[3]	陈连生, 张露友, 田亚强, 杨子旋, 李红斌, 潘红波, 魏英立. 低碳高强舰船用钢的CCT曲线及其组织性能[J]. 金属热处理, 2022, 47(4): 63-68.
[4]	王琪, 吴光亮. 回火温度对1100 MPa级高强钢组织与性能的影响[J]. 金属热处理, 2022, 47(4): 146-150.
[5]	孙凯, 陈研, 杨绍斌. 时效温度对激光选区熔化TC21钛合金微观组织及硬度的影响[J]. 金属热处理, 2022, 47(4): 155-158.
[6]	刘文彬, 乔龙阳, 潘新宇, 程格, 李爱娜, 裴新军. 淬火温度对刀剪用M390粉末冶金不锈钢组织和性能的影响[J]. 金属热处理, 2022, 47(4): 189-195.
[7]	王瑞琴, 葛鹏, 廖强, 侯鹏, 刘宇. 固溶冷却方式对短时用高温钛合金板材组织和性能的影响[J]. 金属热处理, 2022, 47(4): 196-198.
[8]	王绍灼, 孟晗, 王芬, 樊海卫, 李燕, 唐超. 改善低氧TC4-LC及重熔TC4钛合金性能的热处理工艺[J]. 金属热处理, 2022, 47(4): 204-207.
[9]	张宁, 高星, 王芝林, 蒋波, 刘雅政. 18CrNiMo7-6钢齿轮组织性能异常分析[J]. 金属热处理, 2022, 47(4): 268-273.
[10]	王敬元, 吴松全, 张博华, 辛社伟, 杨义, 王皞, 黄爱军. 固溶时效处理对BT25y钛合金显微组织及硬度的影响[J]. 金属热处理, 2022, 47(3): 14-19.
[11]	孙建, 黄贞益, 李景辉, 王萍. 固溶和时效处理对Fe-Mn-Al-C轻质钢组织和硬度的影响[J]. 金属热处理, 2022, 47(3): 34-38.
[12]	王方军, 刘应龙, 时瑶, 万红, 刘斌斌. 等温退火处理对Inconel 625合金箔材组织和性能的影响[J]. 金属热处理, 2022, 47(3): 77-81.
[13]	张曼雪, 景然, 张雄, 张晴, 吴倩, 刘以柔. 铸态Ti-20Zr-10Nb-xMo合金的微观组织和耐腐蚀性能[J]. 金属热处理, 2022, 47(3): 147-150.
[14]	宁静, 高坤元, 李浩楠, 文胜平, 黄晖, 吴晓蓝, 魏午, 聂祚仁. 成分和冷却速度对Al-xEr合金凝固组织的影响[J]. 金属热处理, 2022, 47(3): 151-154.
[15]	王荣, 龚玉辉, 殷学俊, 魏德强. 多道电子束扫描搭接率对40Cr钢组织与性能的影响[J]. 金属热处理, 2022, 47(3): 191-197.