金属热处理 ›› 2021, Vol. 46 ›› Issue (6): 177-185.DOI: 10.13251/j.issn.0254-6051.2021.06.035

• 组织与性能 • 上一篇    下一篇

固溶温度对GH4720Li合金显微组织和力学性能的影响

唐超1,2, 张筱萌2, 罗俊鹏3, 曲敬龙1,2, 杜金辉1,2, 张继1,2   

  1. 1.钢铁研究总院 高温材料研究所, 北京 100081;
    2.北京钢研高纳科技股份有限公司, 北京 100081;
    3.中国航发南方工业有限公司, 湖南 株洲 412002
  • 收稿日期:2021-03-10 出版日期:2021-06-25 发布日期:2021-07-21
  • 作者简介:唐 超(1988—),男,工程师,博士,主要研究方向为变形高温合金,E-mail:tagnchao5543@163.com。
  • 基金资助:
    国家自然科学基金(52074092)

Effect of solution temperature on microstructure and mechanical properties of GH4720Li alloy

Tang Chao1,2, Zhang Xiaomeng2, Luo Junpeng3, Qu Jinglong1,2, Du Jinhui1,2, Zhang Ji1,2   

  1. 1. High Temperature Material Research Institute, Central Iron and Steel Research Institute, Beijing 100081, China;
    2. Gaona Aero Material Co., Ltd., Beijing 100081, China;
    3. AECC South Industry Co., Ltd., Zhuzhou Hunan 412002, China
  • Received:2021-03-10 Online:2021-06-25 Published:2021-07-21

摘要: 通过光学显微镜、场发射电镜和力学性能测试,研究了固溶温度对GH4720Li合金显微组织(晶粒、γ′相)及力学性能的影响。结果表明:随着固溶温度的升高,一次γ′相含量减少,三次γ′相尺寸增大,晶粒长大的趋势也变得明显。当固溶温度超过1120 ℃后,一次γ′相回溶迅速,晶粒长大迅速,晶粒尺寸分布不均匀性增加。固溶温度与强度呈抛物线性关系,在1130 ℃强度出现峰值;固溶温度的升高,合金塑性下降,固溶温度超过1100 ℃时塑性下降得更快。680 ℃/830 MPa持久拉伸试验表明,随着固溶温度的提高,持久时间增加,当固溶温度超过1100 ℃持久时间增加明显,但超过1130 ℃持久时间基本不变;随着固溶温度的提高,持久塑性下降,但在1110 ℃之前下降缓慢,超过该温度塑性降低很快,甚至不达标。并讨论了固溶温度-组织-力学性能之间的关联性,该结果为GH4720Li合金盘件的固溶热处理工艺的选择提供了理论参考。

关键词: GH4720Li合金, 固溶温度, 晶粒组织, γ′相, 力学性能

Abstract: Effect of solution temperature on microstructure (including grain and γ′ phase) and mechanical properties of the GH4720Li alloy was investigated by means of optical microscope(OM), field emission scanning electron microscope(FESEM) and mechanical tensile tester. The results show that the volume fraction of primary γ′ decreases, the diameter of tertiary γ′ increases and the average grain size increases with the solution temperature increasing. When the solid solution temperature exceeds 1120 ℃, the primary γ′ phase is rapidly dissolved, the grain grows rapidly, the grain size distribution inhomogeneity increases. The solid solution temperature has a parabolic linear relationship with the strength, and the strength peak is at 1130 ℃. As the solution temperature increases, the plasticity of the alloy decreases, and when the solution temperature exceeds 1100 ℃, the plasticity decreases faster. Stress-rupture tensile test under 680 ℃/830 MPa shows that the duration increases with the increase of solid solution temperature; when the solution temperature exceeds 1100 ℃, the duration increases obviously, but when the solution temperature exceeds 1130 ℃, the duration remains basically unchanged. As the solution temperature increases, the persistent plasticity decreases, but it decreases slowly below 1110 ℃, and rapidly or is even substandard above 1110 ℃. Furthermore, the relationship between solid solution temperature, microstructure and mechanical properties is discussed. The results provide a theoretical reference for the selection of solid solution heat treatment process for GH4720Li alloy disc.

Key words: GH4720Li alloy, solution temperature, grain structure, γ′ phase, mechanical properties

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