金属热处理 ›› 2024, Vol. 49 ›› Issue (2): 98-103.DOI: 10.13251/j.issn.0254-6051.2024.02.015

• 工艺研究 • 上一篇    下一篇

不同热处理工艺对9Ni低温容器用钢组织与性能的影响

李铖1, 彭其春1, 童志博2, 梁亮3, 齐江华3, 肖爱达3, 董常福3   

  1. 1.武汉科技大学 耐火材料与冶金国家重点实验室, 湖北 武汉 430081;
    2.长江师范学院 材料科学与工程学院, 重庆 408100;
    3.湖南华菱涟源钢铁有限公司技术中心, 湖南 娄底 417009
  • 收稿日期:2023-08-30 修回日期:2024-01-07 出版日期:2024-03-27 发布日期:2024-03-27
  • 通讯作者: 彭其春,教授,硕士生导师,E-mail:pengqichun1964@163.com
  • 作者简介:李 铖(1999—),男,硕士研究生,主要研究方向为低温容器钢的组织与性能,E-mail:lc13040929388@163.com。

Effects of different heat treatment processes on microstructure and properties of 9Ni cryogenic vessel steel

Li Cheng1, Peng Qichun1, Tong Zhibo2, Liang Liang3, Qi Jianghua3, Xiao Aida3, Dong Changfu3   

  1. 1. The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan Hubei 430081, China;
    2. College of Materials Science and Engineering, Yangtze Normal University, Chongqing 408100, China;
    3. Technology Center of Lianyuan Iron & Steel Co., Ltd., Loudi Hunan 417009, China
  • Received:2023-08-30 Revised:2024-01-07 Online:2024-03-27 Published:2024-03-27

摘要: 研究了QT和QLT两种热处理工艺对9Ni钢力学性能的影响规律,并探讨了其韧化机理。结果表明,QT和QLT处理对9Ni钢的力学性能影响明显,并且对比QT处理试样,QLT处理试样的抗拉强度和屈服强度有所下降,伸长率小幅度提高,但其低温冲击性能增加显著,增加了近40 J。QT处理试样具有典型韧性断裂特征,其冲击断口附近,存在较粗大马氏体组织,偏聚带主要为板条状马氏体,且板条之间呈现出多边化的趋势,组织中存在一定量的亮衬区域,主要为回火过程中形成的逆转变奥氏体,能明显改善9Ni钢的低温韧性。而QLT处理试样板条状马氏体更为细小和均匀,在板条间隙亮衬区域分布更为广泛,其低温冲击后试样存在更多尺寸较小且分布均匀的韧窝。低温冲击试验后QT和QLT处理试样的逆转变奥氏体体积分数分别为0.88%和6.60%,因此QLT处理试样的低温韧性较好,而逆转变奥氏体吸收了基体中固溶强化元素后,导致屈服强度降低。

关键词: 9Ni钢, 调质处理, 两相区热处理, 显微组织, 低温韧性

Abstract: Effects of QT and QLT treatments on mechanical properties of the 9Ni steel were studied, and the toughening mechanism was discussed. The results show that QT and QLT treatments have a significant impact on the mechanical properties of 9Ni steel. Compared with QT treated specimen, the tensile strength and yield strength of the specimen treated by QLT are decreased, but the elongation is increased slightly, the low temperature impact property is increased significantly by nearly 40 J. QT treated specimen has typical ductile fracture characteristics. There is a coarse martensite structure near the impact fracture. The segregation zone is mainly lath martensite, and there is a trend of multilateralization between martensitic lath. There is a certain amount of bright areas in the structure, which are mainly reversed austenite formed during tempering, and can significantly improve the low temperature toughness of the 9Ni steel. However, the lath martensite of the QLT treated specimen is finer and more uniform, there are more bright areas between the martensitic lath, and the specimen after low-temperature impact test has more dimples with smaller size and uniform distribution. After low temperature impact test, the volume fraction of reversed austenite in QT and QLT treated specimens is 0.88% and 6.60%, respectively, therefore the low temperature toughness of the QLT treated specimen is better, while the reversed austenite absorbs the solid solution strengthening elements in the substrate, resulting in the reduction of yield strength.

Key words: 9Ni steel, quenching and tempering treatment, quenching, intercritical quenching and tempering, microstructure, low temperature toughness

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