金属热处理 ›› 2023, Vol. 48 ›› Issue (5): 241-245.DOI: 10.13251/j.issn.0254-6051.2023.05.037

• 工艺研究 • 上一篇    下一篇

大型轧机拉杆离子氮碳共渗+后氧化复合工艺

房颖, 李博, 李双喜   

  1. 河南机电职业学院 汽车工程学院, 河南 郑州 451191
  • 收稿日期:2022-10-23 修回日期:2023-03-13 出版日期:2023-05-25 发布日期:2023-06-21
  • 通讯作者: 李双喜,高级工程师,博士,E-mail: 15890605077@163.com
  • 作者简介:房 颖(1981—),女,副教授,硕士,主要研究方向为汽车制造技术,E-mail: 547544173@qq.com。
  • 基金资助:
    河南省科技攻关(222102220029)

Ion nitrocarburizing+post-oxidation combined process for tie rods of large rolling mill

Fang Ying, Li Bo, Li Shuangxi   

  1. Automotive Engineering Institute, Henan Mechanical and Electrical Vocational College, Zhengzhou Henan 451191, China
  • Received:2022-10-23 Revised:2023-03-13 Online:2023-05-25 Published:2023-06-21

摘要: 针对东南亚沿海地区使用的大型轧钢机拉杆(材料为42CrMo钢)易发生腐蚀磨损的问题,采用单热源脉冲离子渗氮炉对拉杆进行氮碳共渗+后氧化复合处理。通过对模拟试样的预氧化工艺、氮碳共渗工艺及后氧化工艺的研究,得到了满足产品要求的复合处理工艺:350 ℃×2 h预氧化;550 ℃×24 h氮碳共渗(炉压为260 Pa,NH3∶CO2=20∶1)和520 ℃×2 h氮氧共渗(炉压为300 Pa,NH3∶O2=6∶1),共渗完毕,关闭电源,同时以0.5 L/min向炉内通入空气,直至炉温降到300 ℃,打开炉盖,待试样冷至150 ℃左右,迅速在试样表面均匀涂上防锈油。在此复合工艺下,渗层深度达到0.39~0.41 mm,化合物层达到10~12 μm,与同工艺无预氧化试样渗层及化合物层厚度相比均增加;经盐雾试验检测,试样在70 h后出现腐蚀斑,和只经氮碳共渗处理无后氧化处理相比,耐蚀性提高。

关键词: 大型轧机, 拉杆, 42CrMo钢, 离子氮碳共渗, 后氧化, 耐蚀性

Abstract: Aiming to avoid the corrosion and wear problem of the 42CrMo steel tie rods of large rolling mill used in the coastal areas of Southeast Asia, nitrocarburizing and post-oxidation combined treatment was carried out by using a single heat source pulsed ion nitriding furnace. The research results on the pre-oxidation, nitrocarburizing and post-oxidation processes of the simulated specimen show that, the combined treatment process which meets the product requirements is: firstly pre-oxidation at 350 ℃ for 2 h in air furnace, secondly, nitrocarburizing at 550 ℃ for 24 h (furnace pressure of 260 Pa, NH3∶CO2 ratio of 20∶1), thirdly, post-oxidation at 520 ℃ for 2 h (furnace pressure of 300 Pa, NH3∶O2 of 6∶1), then turning the power and penetrating agent off and introducing air into the furnace at a speed of 0.5 L/min until the furnace temperature dropping to 300 ℃, finally, quickly and evenly coating the surface of the specimen with anti-rust oil when the specimen cooled to about 150 ℃. Under this combined process, the depth of the infiltration layer reaches 0.39-0.41 mm, the compound layer reaches 10-12 μm, which is thicker than that under the same process without pre-oxidation. After salt spray testing, corrosion spots appear on the specimen only until 70 h, and the corrosion resistance is higher than that only undergoing nitrocarburizing treatment without post-oxidation treatment.

Key words: large rolling mill, tie rod, 42CrMo steel, ion nitrocarburizing, post-oxidation, corrosion resistance

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