金属热处理 ›› 2025, Vol. 50 ›› Issue (6): 12-17.DOI: 10.13251/j.issn.0254-6051.2025.06.003

• 材料研究 • 上一篇    下一篇

LNG储罐用9%Ni钢模拟热变形过程的静态再结晶行为

帅勇1, 孙乐飞1, 董富军1, 操瑞宏1, 万勇2, 刘明启2, 温永红2   

  1. 1.新余钢铁股份有限公司, 江西 新余 338000;
    2.安徽工业大学 冶金工程学院, 安徽 马鞍山 243002
  • 收稿日期:2024-12-17 修回日期:2025-03-23 出版日期:2025-06-25 发布日期:2025-07-08
  • 通讯作者: 孙乐飞,高级工程师,博士,E-mail:slf@xinsteel.com.cn
  • 作者简介:帅 勇(1983—),男,高级工程师,博士,主要研究方向为炼钢工艺控制及管理,E-mail:shy@xinsteel.com.cn。
  • 基金资助:
    江西省赣鄱俊才支持计划(20243BCE51032)

Static recrystallization behavior of 9%Ni steel for LNG storage tank during simulating hot deformation

Shuai Yong1, Sun Lefei1, Dong Fujun1, Cao Ruihong1, Wan Yong2, Liu Mingqi2, Wen Yonghong2   

  1. 1. Xinyu Iron and Steel Co., Ltd., Xinyu Jiangxi 338000, China;
    2. School of Metallurgical Engineering, Anhui University of Technology, Ma'anshan Anhui 243002, China
  • Received:2024-12-17 Revised:2025-03-23 Online:2025-06-25 Published:2025-07-08

摘要: 通过Gleeble-3800热模拟试验机和Leica显微镜研究了压缩温度(950~1050 ℃)和道次间隔时间(1~120 s)对9%Ni钢热压缩期间静态再结晶行为的影响,并结合真应力-真应变曲线、软化率、静态再结晶体积分数和显微组织,建立了9%Ni钢的静态再结晶激活能和动力学模型。结果显示,随着压缩温度和道次间隔时间的增加,9%Ni钢的软化率、静态再结晶体积分数及再结晶晶粒尺寸均呈现上升趋势。相比延长道次间隔时间,提高压缩温度更有利于促进9%Ni钢热变形后的静态回复和再结晶。为避免9%Ni 钢轧制过程出现混晶组织,其轧制温度若在900~1000 ℃,道次间隔时间应不少于20 s。9%Ni钢的静态再结晶激活能为229 kJ/mol,其静态再结晶动力学模型为$X_{\text {srex }}=1-\exp \left[-0.693\left(\frac{t}{t_{0.5}}\right)^{0.321}\right]$。

关键词: 9%Ni钢, 双道次热压缩, 软化率, 静态再结晶, 动力学模型

Abstract: Effects of compression temperature (950-1050 ℃) and pass interval (1-120 s) on the static recrystallization behavior of 9%Ni steel during hot compression were studied by Gleeble-3800 thermal simulation testing machine and Leica microscope. The static recrystallization activation energy and kinetic model of 9%Ni steel were established. The results show that with the increase of compression temperature and pass interval, the softening rate, static recrystallization volume fraction, and recrystallized grain size of the 9%Ni steel all exhibit an upward trend. The static recovery and recrystallization of the 9%Ni steel after hot deformation can be promoted by increasing the compression temperature compared with extending the pass interval. In order to avoid the mixed grain structure in the rolling process of the 9%Ni steel, the rolling temperature should be in the range of 900-1000 ℃, and the pass interval should be not less than 20 s. The static recrystallization activation energy of the 9%Ni steel is obtained by calculation to be 229 kJ/mol, and its static recrystallization kinetic model is $X_{\text {srex }}=1-\exp \left[-0.693\left(\frac{t}{t_{0.5}}\right)^{0.321}\right]$.

Key words: 9%Ni steel, double pass hot compression, softening rate, static recrystallization, kinetic model

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