Heat Treatment of Metals ›› 2024, Vol. 49 ›› Issue (1): 262-267.DOI: 10.13251/j.issn.0254-6051.2024.01.042

• SURFACE ENGINEERING • Previous Articles     Next Articles

Effect of annealing on porosity of Cr coating on zirconium alloy surface

Li Zhikang1, Wang Quanwei1, Shen Xiaofeng1, Huang Jiao1, Fan Lifeng2, Ma Wen1, Zhang Pengxing3   

  1. 1. Inner Mongolia Key Laboratory of Thin Film and Coatings, School of Materials Science and Engineering, Inner Mongolia University of Technology, Hohhot Inner Mongolia 010051, China;
    2. Engineering Research Center of Rare Earth Metals, Inner Mongolia University of Technology, Hohhot Inner Mongolia 010051, China;
    3. Northwest Institute for Nonferrous Metal Research, Xi'an Shaanxi 710016, China
  • Received:2023-08-18 Revised:2023-11-28 Published:2024-02-29

Abstract: Cr coating was prepared on Zr-4 alloy by supersonic flame spraying (high velocity oxygen fuel, HVOF), annealed at 700 ℃ for 2 h, and oxidized at 1000 ℃ in water vapor environment, and the densities of the coating were measured by a Haus balance density measurement kit to investigate the effect of annealing on the porosity of Cr coatings. The results show that annealing can significantly improve the Cr coating density and compensate for the high porosity of the coating by HVOF with the experimental process parameters. There is no significant change in the interface between the coating and the substrate. The oxidation resistance of the annealed Cr coating is better than that of the unannealed specimen. It indicates that appropriate annealing after coating preparation can enhance the oxidation resistance at high temperature by increasing the coating densities and improving the coating microstructure.

Key words: zircaloy, Cr coating, HVOF, annealing, density

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